Domain coarsening in viscous sintering as a result of topological pore evolution

被引:6
作者
Okuma, Gaku [1 ,2 ]
Tanaka, Satoshi [3 ]
Wakai, Fumihiro [1 ,2 ]
机构
[1] Natl Inst Mat Sci NIMS, Res Ctr Struct Mat, Ibaraki 3050047, Japan
[2] Tokyo Inst Technol, Inst Innovat Res, Lab Mat & Struct Lab, Yokohama, Kanagawa 2268503, Japan
[3] Nagaoka Univ Technol, Dept Mat Sci & Technol, 1603-1 Kamitomioka, Nagaoka, Niigata 16031, Japan
关键词
X-ray microtomography; Topology; Coarsening; Viscous sintering; GRAIN-GROWTH; IN-SITU; SIZE; VISUALIZATION; INTERMEDIATE; STABILITY; KINETICS; DENSITY; STRESS; FLOW;
D O I
10.1016/j.jeurceramsoc.2021.10.013
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
The microstructure evolution in 3D was studied by X-ray microtomography to reveal the relation between topology of pore networks and characteristic length in viscous sintering. The mean intercept length was defined from solid/pore interface for characterizing the length of solid phase and pore phase. The increase of the characteristic length with densification was termed as domain coarsening. The topological pore evolution was analyzed by using genus. The characteristic length increased with decreasing genus in the intermediate stage. The domain coarsening takes place as a natural consequence of pore evolution in viscous sintering, i.e., the decrease of total surface area concurrent with the topological transformations.
引用
收藏
页码:729 / 733
页数:5
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