Microwave Synthesis of Molybdenum Disulfide Nanoparticles Using Response Surface Methodology for Tribological Application

被引：6
作者：
Nagarajan, Thachnatharen [1 ,2 ]
Khalid, Mohammad [2 ,3 ]
Sridewi, Nanthini [1 ]
Jagadish, Priyanka [2 ]
Walvekar, Rashmi [4 ]
机构：
[1] Natl Def Univ Malaysia, Fac Def Sci & Technol, Kuala Lumpur 57000, Malaysia
[2] Sunway Univ, Sch Engn & Technol, Graphene & Adv 2D Mat Res Grp GAMRG, Subang Jaya 47500, Malaysia
[3] Sunway Univ, Sch Engn & Technol, Sunway Mat Smart Sci & Engn SMS2E Res Cluster, Subang Jaya 47500, Malaysia
[4] Xiamen Univ Malaysia, Sch Energy & Chem Engn, Dept Chem Engn, Jalan Sunsuria, Bandar Sunsuria 43900, Sepang, Malaysia
来源：
NANOMATERIALS | 2022年 / 12卷 / 19期
关键词：
microwave synthesis; optimization; MoS2; nanoparticles; nanolubricants; tribology; HYDROTHERMAL SYNTHESIS; MOS2; NANOSHEETS; BEHAVIOR; PERFORMANCE; GROWTH;
D O I：
10.3390/nano12193369
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
We used response surface methodology (RSM) based on the central composite design (CCD) model to optimize the synthesis time and temperature of the molybdenum disulfide (MoS2) nanoparticles using the flexiWAVE microwave. Furthermore, the synthesized MoS2 nanoparticles were used in SAE 20W50 diesel engine oil to study the tribological properties according to ASTM standards using a four-ball tribotester. The optimization result shows that the synthesis temperature and time for the MoS2 nanoparticles in the microwave were similar to 200 degrees C and similar to 15 min, respectively, with a coefficient of friction (COF) and average wear scar diameter (WSD) of 0.0849 and 320 mu m. Furthermore, the difference between the experimental and predicted values was minimal (1.88% (COF) and 0.625% (WSD)), which was similar to the optimization model.
引用
收藏
页数：18
相关论文
共 50 条
  • [31] Synthesis and characterization of molybdenum disulfide nanoparticles inShewanella oneidensisMR-1 biofilms
    Rees, James D.
    Gorby, Yuri A.
    Sawyer, Shayla M.
    BIOINTERPHASES, 2020, 15 (04)
  • [32] Optimization of Sonocatalytic Orange II Degradation on MoS2 Nanoparticles using Response Surface Methodology
    Li, Jiulong
    Ko, Jeong Won
    Ko, Weon Bae
    ELASTOMERS AND COMPOSITES, 2023, 58 (04): : 191 - 200
  • [33] Synthesis of Porous Molybdenum Disulfide Materials with High Specific Surface Area Using Sodium Chloride as the Template
    An, Gaojun
    Xiong, Chunhua
    Lu, Changbo
    Chen, Zhaojun
    HIGH PERFORMANCE STRUCTURES AND MATERIALS ENGINEERING, PTS 1 AND 2, 2011, 217-218 : 1569 - +
  • [34] Composite films based on chitosan incorporating molybdenum disulfide nanosheets and zinc oxide nanoparticles with potential antibacterial application
    Hidayat, Muhammad Iqbal
    Hardiansyah, Andri
    Khoiriah, Khoiriah
    Yulianti, Evi
    Wardhani, Riesca Ayu Kusuma
    Fahrialdi, Fahrialdi
    Yusuf, Muhammad Rayhan Izzati
    FOOD CHEMISTRY, 2025, 477
  • [35] The application of response surface methodology on the synthesis of conductive polyaniline/cellulosic fiber nanocomposites
    Sharifi, Hassan
    Zabihzadeh, Seyed Majid
    Ghorbani, Mohsen
    CARBOHYDRATE POLYMERS, 2018, 194 : 384 - 394
  • [36] Rubbercrete mixture optimization using response surface methodology
    Mohammed, Bashar S.
    Khed, Veerendrakumar C.
    Nuruddin, Muhd Fadhil
    JOURNAL OF CLEANER PRODUCTION, 2018, 171 : 1605 - 1621
  • [37] Effect of Co-Fe alloy nanoparticles on the surface electronic structure of molybdenum disulfide nanosheets and its application as a bifunctional catalyst for rechargeable zinc air battery
    Shang, Xiaonan
    Shen, Qiujie
    Xiong, Yi
    Jiang, Zhongqing
    Qin, Chu
    Tian, Xiaoning
    Yang, Xufeng
    Jiang, Zhong-Jie
    JOURNAL OF ALLOYS AND COMPOUNDS, 2022, 916
  • [38] Application of Response Surface Methodology for the Technological Improvement of Solid Lipid Nanoparticles
    Dal Pizzol, Carine
    Beringhs, Andre O'Reilly
    Winter, Evelyn
    Sonaglio, Diva
    de Campos, Angela Machado
    Creczynski-Pasa, Tania Beatriz
    JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, 2016, 16 (02) : 1238 - 1247
  • [39] Application of Response Surface Methodology on Characteristics of Lubricant with Titanium Oxide Nanoparticles
    Mohamad, Nor Syahirah
    Kasolang, Salmiah
    Abu Bakar, Mimi Azlina
    PROCEEDINGS OF INTERNATIONAL CONFERENCE ON ADVANCED PROCESSES AND SYSTEMS IN MANUFACTURING (APSIM 2016), 2016, : 107 - 108
  • [40] Hydrothermal synthesis of hydroxyapatite powders using Response Surface Methodology (RSM)
    Ebrahimi, Shamsi
    Nasri, Coswald Stephen Sipaut Mohd
    Bin Arshad, Sazmal Effendi
    PLOS ONE, 2021, 16 (05):
12345