Hot deformation of Mg-Y-Zn alloy with a low content of the LPSO phase studied by in-situ synchrotron radiation diffraction

被引:25
作者
Fekete, Klaudia Horvath [1 ,2 ]
Drozdenko, Daria [1 ,3 ]
Capek, Jan [1 ,4 ]
Mathis, Kristian [1 ]
Tolnai, Domonkos [5 ]
Stark, Andreas [5 ]
Garces, Gerardo [6 ]
Dobron, Patrik [1 ,2 ]
机构
[1] Charles Univ Prague, Fac Math & Phys, Dept Phys Mat, Ke Karlovu 5, CR-12116 Prague, Czech Republic
[2] CAS, Nucl Phys Inst, Rez 25068, Czech Republic
[3] Kumamoto Univ, Magnesium Res Ctr, Chuo Ku, 2-39-1 Kurokami, Kumamoto 8608555, Japan
[4] Paul Scherrer Inst, Lab Neutron Scattering & Imaging, CH-5232 Villigen, Switzerland
[5] Helmholtz Zentrum Geesthacht, Inst Mat Sci, Max Planck Str 1, D-21502 Geesthacht, Germany
[6] CENIM CSIC, Dept Phys Met, Ave Gregorio del Amo 8, E-28040 Madrid, Spain
关键词
Magnesium alloy; LPSO phase; Kinking; High temperature; Synchrotron radiation diffraction; STACKING-ORDERED PHASE; NEUTRON-DIFFRACTION; MECHANICAL-PROPERTIES; DYNAMIC RECRYSTALLIZATION; COMPRESSION BEHAVIOR; PLASTIC-DEFORMATION; ACOUSTIC-EMISSION; MAGNESIUM; EVOLUTION; TEMPERATURE;
D O I
10.1016/j.jma.2019.11.009
中图分类号
TF [冶金工业];
学科分类号
0806 ;
摘要
The compressive deformation behavior of the extruded WZ42 (Mg98.5Y1Zn0.5 in at.%) magnesium alloy containing a low amount of long-period stacking ordered (LPSO) phase was studied by in-situ synchrotron radiation diffraction technique. Tests were conducted at temperatures between room temperature and 350 degrees C. Detailed microstructure investigation was provided by scanning electron microscopy, particularly the backscattered electron imaging and electron backscatter diffraction technique. The results show that twinning lost its dominance and kinking of the LPSO phase became more pronounced with increasing deformation temperature. No cracks of the LPSO phase and no debonding r at the interface between the LPSO phase and the Mg matrix were observed at temperatures above 200 degrees C. At 350 degrees C, the LPSO phase lost its strengthening effect and the deformation of the alloy was mainly realized by the dynamic recrystallization of the Mg matrix. (c) 2020 Published by Elsevier B.V. on behalf of Chongqing University.
引用
收藏
页码:199 / 209
页数:11
相关论文
共 48 条
[1]   Polytypes of long-period stacking structures synchronized with chemical order in a dilute Mg-Zn-Y alloy [J].
Abe, E. ;
Ono, A. ;
Itoi, T. ;
Yamasaki, M. ;
Kawamura, Y. .
PHILOSOPHICAL MAGAZINE LETTERS, 2011, 91 (10) :690-696
[2]   Long-period ordered structure in a high-strength nanocrystalline Mg-1 at% Zn-2 at% Y alloy studied by atomic-resolution Z-contrast STEM [J].
Abe, E ;
Kawamura, Y ;
Hayashi, K ;
Inoue, A .
ACTA MATERIALIA, 2002, 50 (15) :3845-3857
[3]   Validating a polycrystal model for the elastoplastic response of magnesium alloy AZ31 using in situ neutron diffraction [J].
Agnew, S. R. ;
Brown, D. W. ;
Tome, C. N. .
ACTA MATERIALIA, 2006, 54 (18) :4841-4852
[4]   In situ neutron diffraction and polycrystal plasticity modeling of a Mg-Y-Nd-Zr alloy: Effects of precipitation on individual deformation mechanisms [J].
Agnew, S. R. ;
Mulay, R. P. ;
Polesak, F. J., III ;
Calhoun, C. A. ;
Bhattacharyya, J. J. ;
Clausen, B. .
ACTA MATERIALIA, 2013, 61 (10) :3769-3780
[5]   A study of the heterogeneity of plastic deformation in IF steel by EBSD [J].
Allain-Bonasso, Nathalie ;
Wagner, Francis ;
Berbenni, Stephane ;
Field, David P. .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2012, 548 :56-63
[6]  
[Anonymous], 2012, GREEN CAR C
[7]   Effect of rare earth elements on the microstructure and texture development in magnesium-manganese alloys during extrusion [J].
Bohlen, Jan ;
Yi, Sangbong ;
Letzig, Dietmar ;
Kainer, Karl Ulrich .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2010, 527 (26) :7092-7098
[8]   Internal strain and texture evolution during deformation twinning in magnesium [J].
Brown, DW ;
Agnew, SR ;
Bourke, MAM ;
Holden, TM ;
Vogel, SC ;
Tomé, CN .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2005, 399 (1-2) :1-12
[9]   Temperature dependence of twinning activity in random textured cast magnesium [J].
Capek, Jan ;
Farkas, Gergely ;
Pilch, Jan ;
Mathis, Kristian .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2015, 627 :333-335
[10]   Study of the loading mode dependence of the twinning in random textured cast magnesium by acoustic emission and neutron diffraction methods [J].
Capek, Jan ;
Mathis, Kristian ;
Clausen, Bjorn ;
Straska, Jitka ;
Beran, Premysl ;
Lukas, Petr .
MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2014, 602 :25-32