Acetyl-d(3) chloride: A convenient nonchiral derivatizing agent (NCDA) for a facile enantiomeric excess determination of amines through deuterium NMR

被引：8

作者：

Canet, JL

Canet, I

Courtieu, J

DaSilva, S

Gelas, J

Troin, Y

机构：

[1] UNIV CLERMONT FERRAND,URA CNRS 485,LAB SYNTH & ETUD SYST INTERNET BIOL,F-63177 CLERMONT FERRAN,FRANCE

[2] UNIV PARIS 11,CHIM ORGAN STRUCT LAB,URA CNRS 1384,ICMO,F-91405 ORSAY,FRANCE

来源：

JOURNAL OF ORGANIC CHEMISTRY | 1996年 / 61卷 / 25期

关键词：

D O I：

10.1021/jo961141f

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

[No abstract available]

引用

页码：9035 / 9037

页数：3

共 7 条

[1] CHIRAL DIAMINES FOR A NEW PROTOCOL TO DETERMINE THE ENANTIOMERIC COMPOSITION OF ALCOHOLS, THIOLS, AND AMINES BY P-31, H-1, C-13, AND F-19 NMR [J].

ALEXAKIS, A ;

FRUTOS, JC ;

MUTTI, S ;

MANGENEY, P .

JOURNAL OF ORGANIC CHEMISTRY, 1994, 59 (12) :3326-3334

[2] CYANOHYDRIDOBORATE ANION AS A SELECTIVE REDUCING AGENT [J].

BORCH, RF ;

BERNSTEIN, MD ;

DURST, HD .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1971, 93 (12) :2897-+

[3] NEW, AND ACCURATE METHOD TO DETERMINE THE ENANTIOMERIC PURITY OF AMINO-ACIDS BASED ON DEUTERIUM NMR IN A CHOLESTERIC LYOTROPIC LIQUID-CRYSTAL [J].

CANET, I ;

MEDDOUR, A ;

COURTIEU, J ;

CANET, JL ;

SALAUN, J .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1994, 116 (05) :2155-2156

[4] ENANTIOMERIC ANALYSIS IN A POLYPEPTIDE LYOTROPIC LIQUID-CRYSTAL BY DEUTERIUM NMR [J].

CANET, I ;

COURTIEU, J ;

LOEWENSTEIN, A ;

MEDDOUR, A ;

PECHINE, JM .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1995, 117 (24) :6520-6526

[5]

HULST R, 1995, RECL TRAV CHIM PAY B, V114, P115

[6] OBSERVATION OF ENANTIOMERS, CHIRAL BY VIRTUE OF ISOTOPIC-SUBSTITUTION, THROUGH DEUTERIUM NMR IN A POLYPEPTIDE LIQUID-CRYSTAL [J].

MEDDOUR, A ;

CANET, I ;

LOEWENSTEIN, A ;

PECHINE, JM ;

COURTIEU, J .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1994, 116 (21) :9652-9656

[7] NMR DETERMINATION OF ENANTIOMERIC PURITY [J].

PARKER, D .

CHEMICAL REVIEWS, 1991, 91 (07) :1441-1457

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