In situ generation of silver nanoparticles in cellulose matrix using Azadirachta indica leaf extract as a reducing agent

被引:35
作者
Kishanji, M. [1 ]
Mamatha, G. [1 ]
Reddy, K. Obi [2 ]
Rajulu, A. Varada [3 ]
Madhukar, K. [1 ]
机构
[1] Osmania Univ, Dept Phys, Hyderabad 500007, Andhra Pradesh, India
[2] Univ South Africa, Dept Phys, Coll Sci, Johannesburg, South Africa
[3] Kalasalingam Univ, Int Res Ctr, Ctr Composite Mat, Anand Nagar, Krishnan Koil, India
关键词
Antibacterial activity; cellulose; in situ generation; silver nanoparticles;
D O I
10.1080/1023666X.2017.1369612
中图分类号
O63 [高分子化学(高聚物)];
学科分类号
070305 ; 080501 ; 081704 ;
摘要
In the present work, silver nanoparticles (AgNPs) were in situ generated in cellulose matrix using leaf extract of Azadirachta indica as a reducing agent. The cellulose/AgNP composite films prepared were characterized by FTIR, X-ray diffraction (XRD), scanning electron microscope, and antibacterial tests. The infrared spectra indicated the association of organic materials with silver nanoparticles to serve as capping agents. Scanning electron micrographs showed that synthesized silver nanoparticles were nearly uniform and spherical in shape with diameter in the range of 61-110nm. XRD confirmed the formation of AgNPs and Ag-O nanoparticles. The nanocomposite films showed good antibacterial activity against Escherichia coli bacteria.
引用
收藏
页码:734 / 740
页数:7
相关论文
共 14 条
[1]   Antidiabetic activity of silver nanoparticles from green synthesis using Lonicera japonica leaf extract [J].
Balan, Kannan ;
Qing, Weixia ;
Wang, Youyou ;
Liu, Xiuhua ;
Palvannan, Thayumanavan ;
Wang, Yong ;
Ma, Fanyi ;
Zhang, Yun .
RSC ADVANCES, 2016, 6 (46) :40162-40168
[2]   Rapid dissolution of cellulose in LiOH/Urea and NaOH/Urea aqueous solutions [J].
Cai, J ;
Zhang, L .
MACROMOLECULAR BIOSCIENCE, 2005, 5 (06) :539-548
[3]   Greener Techniques for the Synthesis of Silver Nanoparticles Using Plant Extracts, Enzymes, Bacteria, Biodegradable Polymers, and Microwaves [J].
Hebbalalu, Deepika ;
Lalley, Jacob ;
Nadagouda, Mallikarjuna N. ;
Varma, Rajender S. .
ACS SUSTAINABLE CHEMISTRY & ENGINEERING, 2013, 1 (07) :703-712
[4]  
Kaplan D. L., 1998, BIOPOLYMERS RENEWABL, P55
[5]   Synthesis of silver nanoparticles using Acalypha indica leaf extracts and its antibacterial activity against water borne pathogens [J].
Krishnaraj, C. ;
Jagan, E. G. ;
Rajasekar, S. ;
Selvakumar, P. ;
Kalaichelvan, P. T. ;
Mohan, N. .
COLLOIDS AND SURFACES B-BIOINTERFACES, 2010, 76 (01) :50-56
[6]   Experimental Investigation of Cellulose/Silver Nanocomposites Using In Situ Generation Method [J].
Muthulakshmi, L. ;
Rajini, N. ;
Nellaiah, H. ;
Kathiresan, T. ;
Jawaid, M. ;
Rajulu, A. Varada .
JOURNAL OF POLYMERS AND THE ENVIRONMENT, 2017, 25 (04) :1021-1032
[7]   Preparation and properties of cellulose nanocomposite films with in situ generated copper nanoparticles using Terminalia catappa leaf extract [J].
Muthulakshmi, L. ;
Rajini, N. ;
Nellaiah, H. ;
Kathiresan, T. ;
Jawaid, M. ;
Rajulu, A. Varada .
INTERNATIONAL JOURNAL OF BIOLOGICAL MACROMOLECULES, 2017, 95 :1064-1071
[8]   The effects of combination of methanolic leaf extract of Azadirachta indica and diminazene diaceturate in the treatment of experimental Trypanosoma brucei brucei infection in rats [J].
Omoja, V. U. ;
Anagi, A. O. ;
Obidike, I. R. ;
Ihedioha, T. E. ;
Umeakuana, P. U. ;
Mhomga, L., I ;
Asuzu, I. U. ;
Anika, S. M. .
ASIAN PACIFIC JOURNAL OF TROPICAL MEDICINE, 2011, 4 (05) :337-341
[9]   Antimicrobial Polymers with Metal Nanoparticles [J].
Palza, Humberto .
INTERNATIONAL JOURNAL OF MOLECULAR SCIENCES, 2015, 16 (01) :2099-2116
[10]   Preparation and properties of cellulose/silver nanoparticle composites with in situ-generated silver nanoparticles using Ocimum sanctum leaf extract [J].
Sadanand, V. ;
Rajini, N. ;
Satyanarayana, B. ;
Rajulu, A. Varada .
INTERNATIONAL JOURNAL OF POLYMER ANALYSIS AND CHARACTERIZATION, 2016, 21 (05) :408-416