Validation of the analytical procedure for the determination of polyaromatic hydrocarbons in smoke flavourings using high performance liquid chromatography coupled to an ultraviolet, diode array or fluorescence detector

被引：29
作者：
Brasseur, Catherine
Brose, Francois
Pirlot, Alain
Douny, Caroline
Eppe, Gauthier
Maghuin-Rogister, Guy
Scippo, Marie-Louise
机构：
[1] Univ Liege, Ctr Anal Residues Traces, Dept Food Sci, Lab Food Anal, B-4000 Liege, Belgium
[2] Ctr Anal Residues Traces, Lab Mass Spectrometry, B-4000 Liege, Belgium
来源：
ACCREDITATION AND QUALITY ASSURANCE | 2007年 / 12卷 / 10期
关键词：
polyaromatic hydrocarbons; PAH; HPLC; UV; FLD; smoke flavouring; analytical procedure validation; accuracy profile; uncertainty measurement;
D O I：
10.1007/s00769-007-0295-0
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
High performance liquid chromatography (HPLC) coupled to an ultraviolet (UV), diode array or fluorescence detector (UV/DAD/FLD) has been used to set up an analytical procedure for the quantification of 16 EU priority polyaromatic hydrocarbons (PAHs) in smoke flavourings. The following parameters have been determined for the 16 EU priority PAHs: limit of detection, limit of quantification, precision (repeatability and intermediate precision), recovery and measurement uncertainty, using the concept of accuracy profiles. They were in close agreement with quality criteria described in the Commission Regulation (EC) no. 627/2006 concerning PAHs in smoke flavourings.
引用
收藏
页码：535 / 542
页数：8
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