Sensitive Determination of Gliclazide in Tablets and Urine Using Modified Screen-Printed Electrodes

被引：1

作者：

Tajik, Somayeh ^{[1
]}

Mohammadi, Sayed Zia ^{[2
]}

Beitollahi, Hadi ^{[3
]}

机构：

[1] Bam Univ Med Sci, NanoBioElectrochem Res Ctr, Bam, Iran

[2] Payame Noor Univ, Dept Chem, Tehran, Iran

[3] Grad Univ Adv Technol, Inst Sci & High Technol & Environm Sci, Dept Environm, Kerman, Iran

来源：

PORTUGALIAE ELECTROCHIMICA ACTA | 2021年 / 39卷 / 04期

关键词：

Gliclazide determination; magnetic core shell nanoparticles; screen-printed carbon electrode; voltammetry; VOLTAMMETRIC DETERMINATION; HPLC METHOD; CARBON; NANOPARTICLES;

D O I：

10.4152/pea.2021390404

中图分类号：

O646 [电化学、电解、磁化学];

学科分类号：

081704 ;

摘要：

In the present work, a simple and low-cost protocol for determination of gliclazide using modified screen-printed electrodes (SPE) was reported. The immobilization of magnetic core-shell manganese ferrite nanoparticles (MCSNP) onto SPE provides a unique opportunity for charge transfer process. Consequently, the electroanalytical sensing of gliclazide was explored at the modified SPE surface. The response of the modified electrode was linear, in the concentration range from 0.5 to 300.0 mu M, and a detection limit of 100 nM was obtained. The proposed method was successfully employed for gliclazide determination in pharmaceutical and human urine samples. The method showed tremendous reproducibility and intra- and inter-day stability, and has proved to be highly reliable for gliclazide analysis in clinical samples.

引用

页码：265 / 275

页数：11

共 39 条

[1] Controlling of systemic absorption of gliclazide through incorporation into alginate beads
Al-Kassas, Raida S.
Al-Gohary, Omaimah M. N.
Al-Faadhel, Monirah M.
[J]. INTERNATIONAL JOURNAL OF PHARMACEUTICS, 2007, 341 (1-2) : 230 - 237
[2] Baghel US, 2012, ASIAN PACIFIC J TROP, V2, pS756
[3] Forced degradation study on gliclazide and application of validated stability-indicating HPLC-UV method in stability testing of gliclazide tablets
Bansal, Gulshan
Singh, Manjeet
Jindal, Kaur Chand
[J]. CHROMATOGRAPHIA, 2007, 66 (9-10) : 751 - 755
[4] Bard AJ., 2001, electrochemical methods: fundamentals and applications, 2nd Edition, V2
[5] Cogrinding as an approach to enhance dissolution rate of a poorly water-soluble drug (gliclazide)
Barzegar-Jalali, Mohammad
Valizadeh, Hadi
Shadbad, Mohammad-Reza Siahi
Adibkia, Khosro
Mohammadi, Ghobad
Farahani, Amin
Arash, Zeynab
Nokhodchi, Ali
[J]. POWDER TECHNOLOGY, 2010, 197 (03) : 150 - 158
[6] Voltammetric determination of 6-thioguanine and folic acid using a carbon paste electrode modified with ZnO-CuO nanoplates and modifier
Beitollahi, Hadi
Ivari, Susan Ghofrani
Torkzadeh-Mahani, Masoud
[J]. MATERIALS SCIENCE & ENGINEERING C-MATERIALS FOR BIOLOGICAL APPLICATIONS, 2016, 69 : 128 - 133
[7] Nanomolar and Selective Determination of Epinephrine in the Presence of Norepinephrine Using Carbon Paste Electrode Modified with Carbon Nanotubes and Novel 2-(4-Oxo-3-phenyl-3,4-dihydroquinazolinyl)-N′-phenyl-hydrazinecarbothioamide
Beitollahi, Hadi
Karimi-Maleh, Hassan
Khabazzadeh, Hojatollah
[J]. ANALYTICAL CHEMISTRY, 2008, 80 (24) : 9848 - 9851
[8] Fabrication of graphene/gold-modified screen-printed electrode for detection of carcinoembryonic antigen
Chan, K. F.
Lim, H. N.
Shams, N.
Jayabal, S.
Pandikumar, A.
Huang, N. M.
[J]. MATERIALS SCIENCE & ENGINEERING C-MATERIALS FOR BIOLOGICAL APPLICATIONS, 2016, 58 : 666 - 674
[9] Core/shell nanoparticles in biomedical applications
Chatterjee, Krishnendu
Sarkar, Sreerupa
Rao, K. Jagajjanani
Paria, Santanu
[J]. ADVANCES IN COLLOID AND INTERFACE SCIENCE, 2014, 209 : 8 - 39
[10] Functionalization of gold screen printed electrodes with bacterial photosynthetic reaction centers by laser printing technology for mediatorless herbicide biosensing
Chatzipetrou, M.
Milano, F.
Giotta, L.
Chirizzi, D.
Trotta, M.
Massaouti, M.
Guascito, M. R.
Zergioti, I.
[J]. ELECTROCHEMISTRY COMMUNICATIONS, 2016, 64 : 46 - 50

← 1 2 3 4 →