An overview of laboratory performance studies conducted by the IAEA for marine pollution studies of metals and organic contaminants

被引:4
作者
de Mora, Stephen
Villeneuve, Jean-Pierre
Wyse, Eric
机构
[1] Aromed Environm Consulting Serv Inc, Kingston, ON K7M 8C2, Canada
[2] Pacific Marine Environm Lab, Int Atom Energy Agcy, MC-98000 Monaco, Monaco
关键词
quality control; quality assurance; intercomparison exercises; reference materials; trace metals; organic compounds; PAHs; PCBs;
D O I
10.1007/s00769-007-0317-y
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
Aspects of the International Atomic Energy Agency (IAEA) Analytical Quality Control Services (AQCS) for marine environmental studies are discussed, focusing on recent laboratory performance studies (LPS) and the production of reference materials for trace metals and organic compounds in various marine matrices. The IAEA has organized seventeen global interlaboratory studies for a range of organic contaminants. Of note has been the inclusion of numerous polychlorinated biphenyl congeners (PCBs) and some sterols of anthropogenic origin. Concurrently, there have been eleven worldwide intercomparison exercises for trace metals in the marine environment, most of which included methylmercury. Although such interlaboratory studies can help improve performance in individual laboratories and regional laboratory networks, the results reveal that problems remain in the determination of some metals and many organic contaminants.
引用
收藏
页码:587 / 592
页数:6
相关论文
共 26 条
[1]  
ASMUND G, 2000, CHEMOSPHERE, V245, P203
[2]  
CARVALHO F. P., 2001, INT J ENVIRON STUD, V58, P139
[3]   Determination of organochlorine compounds, petroleum hydrocarbons, and sterols in a sediment sample, IAEA-383. Results of an intercomparison exercise [J].
Carvalho, FP ;
Villeneuve, JP ;
Cattini, C .
INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 1999, 75 (04) :315-329
[4]   Analytical intercomparison exercises and harmonization within environmental laboratories from developing countries [J].
Carvalho, FP ;
Villeneuve, JP ;
Coquery, M .
INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY, 1999, 74 (1-4) :263-274
[5]   The determination of organochlorine compounds and petroleum hydrocarbons in a seaweed sample: results of a worldwide intercomparison exercise [J].
Carvalho, FP ;
Villeneuve, JP ;
Cattini, C .
TRAC-TRENDS IN ANALYTICAL CHEMISTRY, 1999, 18 (11) :656-664
[6]  
CARVALHO FP, 1998, IAEA B, V40, P7
[7]   A new model for the inference of population characteristics from experimental data using uncertainties. Application to interlaboratory studies [J].
Cofino, WP ;
van Stokkum, IHM ;
Wells, DE ;
Ariese, F ;
Wegener, JWM ;
Peerboom, RAL .
CHEMOMETRICS AND INTELLIGENT LABORATORY SYSTEMS, 2000, 53 (1-2) :37-55
[8]   Certification of trace and major elements and methylmercury concentrations in a macroalgae (Fucus sp.) reference material, IAEA-140 [J].
Coquery, M ;
Carvalho, FP ;
Azemard, S ;
Bachelez, M ;
Horvat, M .
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 2000, 366 (08) :792-801
[9]   The IAEA worldwide intercomparison exercises (1990-1997): determination of trace elements in marine sediments and biological samples [J].
Coquery, M ;
Carvalho, FP ;
Azemard, S ;
Horvat, M .
SCIENCE OF THE TOTAL ENVIRONMENT, 1999, 238 :501-508
[10]   Developments in the use of chromatographic techniques in marine laboratories for the determination of halogenated contaminants and polycyclic aromatic hydrocarbons [J].
de Boer, J ;
Law, RJ .
JOURNAL OF CHROMATOGRAPHY A, 2003, 1000 (1-2) :223-251