Experimental design;
Iron oxide nanoparticles;
Chemical co-precipitation;
MAGNETITE NANOPARTICLES;
LEPIDOCROCITE GAMMA;
AKAGANEITE BETA;
FERRIHYDRITE;
FEOOH;
TRANSFORMATION;
SPECTROSCOPY;
HEMATITE;
GOETHITE;
SPECTRA;
D O I:
10.1007/s13538-018-0616-2
中图分类号:
O4 [物理学];
学科分类号:
0702 ;
摘要:
Magnetic iron oxide nanoparticles have been widely studied for technological and biomedical applications due to its small size and the possibility of functionalizing the surface with intended molecules. Magnetite is the most used phase because of superparamagnetic characteristic, and it is synthesized by co-precipitation, starting from ferrous and ferric ions in alkaline media. However, depending on parameters of chemical reactions, such as molar ratio between iron and hydroxyl groups, stirring rate, and temperature, different iron oxide structures are formed through distinct pathways. Since several variables can affect the size, chemical composition, and crystalline structure of iron oxide nanoparticles during the synthesis, it is very important to apply experimental routines with a well-defined protocol and planning practical steps can significantly improve the quality of products. Plackett-Burman methodology from design of experiments is a filtration analysis, used in the initial stages of a process to investigate the main effects of factors over a characteristic of the final material. In this work, Plackett-Burman technique was employed in order to optimize bare iron oxide nanoparticle production by co-precipitation method, relating the different crystalline phases produced to the experimental routine. Dynamic light scattering, Fourier transform infrared spectroscopy, and X-ray diffractometry were used to characterize the samples.
机构:
Korea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South KoreaKorea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South Korea
Ahn, Taebin
Kim, Jong Hun
论文数: 0引用数: 0
h-index: 0
机构:
Korea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South KoreaKorea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South Korea
Kim, Jong Hun
Yang, Hee-Man
论文数: 0引用数: 0
h-index: 0
机构:
Korea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South KoreaKorea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South Korea
Yang, Hee-Man
Lee, Jeong Woo
论文数: 0引用数: 0
h-index: 0
机构:
Korea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South KoreaKorea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South Korea
Lee, Jeong Woo
Kim, Jong-Duk
论文数: 0引用数: 0
h-index: 0
机构:
Korea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South Korea
Korea Adv Inst Sci & Technol, Ctr Energy & Environm Engn, Taejon 305701, South KoreaKorea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South Korea
机构:
Cornell Univ, Dept Mat Sci & Engn, Ithaca, NY 14853 USACornell Univ, Dept Mat Sci & Engn, Ithaca, NY 14853 USA
Asenath-Smith, Emily
Estroff, Lara A.
论文数: 0引用数: 0
h-index: 0
机构:
Cornell Univ, Dept Mat Sci & Engn, Ithaca, NY 14853 USA
Cornell Univ, Kavli Inst Cornell Nanoscale Sci, Ithaca, NY 14853 USACornell Univ, Dept Mat Sci & Engn, Ithaca, NY 14853 USA
机构:
Univ New S Wales, Sch Civil & Environm Engn, UNSW Sydney New South Wales, Sydney, NSW 2052, AustraliaUniv New S Wales, Sch Civil & Environm Engn, UNSW Sydney New South Wales, Sydney, NSW 2052, Australia
Boland, Daniel D.
Collins, Richard N.
论文数: 0引用数: 0
h-index: 0
机构:
Univ New S Wales, Sch Civil & Environm Engn, UNSW Sydney New South Wales, Sydney, NSW 2052, AustraliaUniv New S Wales, Sch Civil & Environm Engn, UNSW Sydney New South Wales, Sydney, NSW 2052, Australia
Collins, Richard N.
Miller, Christopher J.
论文数: 0引用数: 0
h-index: 0
机构:
Univ New S Wales, Sch Civil & Environm Engn, UNSW Sydney New South Wales, Sydney, NSW 2052, AustraliaUniv New S Wales, Sch Civil & Environm Engn, UNSW Sydney New South Wales, Sydney, NSW 2052, Australia
Miller, Christopher J.
Glover, Chris J.
论文数: 0引用数: 0
h-index: 0
机构:
Australian Synchrotron, Clayton, Vic 3168, AustraliaUniv New S Wales, Sch Civil & Environm Engn, UNSW Sydney New South Wales, Sydney, NSW 2052, Australia
Glover, Chris J.
Waite, T. David
论文数: 0引用数: 0
h-index: 0
机构:
Univ New S Wales, Sch Civil & Environm Engn, UNSW Sydney New South Wales, Sydney, NSW 2052, AustraliaUniv New S Wales, Sch Civil & Environm Engn, UNSW Sydney New South Wales, Sydney, NSW 2052, Australia
机构:
Tunceli Univ, Fac Engn, Dept Environm Engn, TR-62000 Tunceli, TurkeyTunceli Univ, Fac Engn, Dept Environm Engn, TR-62000 Tunceli, Turkey
Demir, Veysel
Ates, Mehmet
论文数: 0引用数: 0
h-index: 0
机构:
Tunceli Univ, Fac Engn, Dept Bioengn, TR-62000 Tunceli, Turkey
Jackson State Univ, Dept Chem & Biochem, Jackson, MS 39217 USATunceli Univ, Fac Engn, Dept Environm Engn, TR-62000 Tunceli, Turkey
Ates, Mehmet
Arslan, Zikri
论文数: 0引用数: 0
h-index: 0
机构:
Jackson State Univ, Dept Chem & Biochem, Jackson, MS 39217 USATunceli Univ, Fac Engn, Dept Environm Engn, TR-62000 Tunceli, Turkey
Arslan, Zikri
Camas, Mustafa
论文数: 0引用数: 0
h-index: 0
机构:
Tunceli Univ, Fac Engn, Dept Bioengn, TR-62000 Tunceli, TurkeyTunceli Univ, Fac Engn, Dept Environm Engn, TR-62000 Tunceli, Turkey
Camas, Mustafa
Celik, Fatih
论文数: 0引用数: 0
h-index: 0
机构:
Tunceli Univ, Fac Engn, Dept Bioengn, TR-62000 Tunceli, TurkeyTunceli Univ, Fac Engn, Dept Environm Engn, TR-62000 Tunceli, Turkey
Celik, Fatih
Bogatu, Corneliu
论文数: 0引用数: 0
h-index: 0
机构:
Jackson State Univ, Dept Civil & Environm Engn, Jackson, MS 39217 USATunceli Univ, Fac Engn, Dept Environm Engn, TR-62000 Tunceli, Turkey
Bogatu, Corneliu
Can, Safak Seyhaneyildiz
论文数: 0引用数: 0
h-index: 0
机构:
Tunceli Univ, Fac Engn, Dept Bioengn, TR-62000 Tunceli, TurkeyTunceli Univ, Fac Engn, Dept Environm Engn, TR-62000 Tunceli, Turkey
机构:
Univ La Rochelle, CNRS, Littoral Environm Soc, UMR 6250, F-17000 La Rochelle, France
CNRS, FR 3097, F-75700 Paris, FranceUniv La Rochelle, Lab Etude Mat Milieu Agressif, EA3167, F-17042 La Rochelle 01, France
Gilbert, Francoise
Refait, Philippe
论文数: 0引用数: 0
h-index: 0
机构:
Univ La Rochelle, Lab Etude Mat Milieu Agressif, EA3167, F-17042 La Rochelle 01, France
CNRS, FR 3097, F-75700 Paris, FranceUniv La Rochelle, Lab Etude Mat Milieu Agressif, EA3167, F-17042 La Rochelle 01, France
Refait, Philippe
Leveque, Francoiss
论文数: 0引用数: 0
h-index: 0
机构:
Univ La Rochelle, CNRS, Littoral Environm Soc, UMR 6250, F-17000 La Rochelle, France
CNRS, FR 3097, F-75700 Paris, FranceUniv La Rochelle, Lab Etude Mat Milieu Agressif, EA3167, F-17042 La Rochelle 01, France
Leveque, Francoiss
Remazeilles, Celine
论文数: 0引用数: 0
h-index: 0
机构:
Univ La Rochelle, Lab Etude Mat Milieu Agressif, EA3167, F-17042 La Rochelle 01, France
CNRS, FR 3097, F-75700 Paris, FranceUniv La Rochelle, Lab Etude Mat Milieu Agressif, EA3167, F-17042 La Rochelle 01, France
Remazeilles, Celine
Conforto, Egle
论文数: 0引用数: 0
h-index: 0
机构:
Univ La Rochelle, Ctr Commun Analyse, F-17071 La Rochelle 09, France
CNRS, FR 3097, F-75700 Paris, FranceUniv La Rochelle, Lab Etude Mat Milieu Agressif, EA3167, F-17042 La Rochelle 01, France
机构:
Sorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, FranceSorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, France
Guyodo, Yohan
Bonville, Pierre
论文数: 0引用数: 0
h-index: 0
机构:
Univ Paris Saclay, CEA Saclay, Serv Phys Etat Condense, CEA,CNRS, Gif Sur Yvette, FranceSorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, France
Bonville, Pierre
Till, Jessica L.
论文数: 0引用数: 0
h-index: 0
机构:
Sorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, France
Deutsch GeoForsch Zentrum, Potsdam, GermanySorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, France
Till, Jessica L.
Ona-Nguema, Georges
论文数: 0引用数: 0
h-index: 0
机构:
Sorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, FranceSorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, France
Ona-Nguema, Georges
Lagroix, France
论文数: 0引用数: 0
h-index: 0
机构:
Sorbonne Paris Cite, UPD, CNRS UMR 7154, Inst Phys Globe Paris, Paris, FranceSorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, France
Lagroix, France
Menguy, Nicolas
论文数: 0引用数: 0
h-index: 0
机构:
Sorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, FranceSorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, France
机构:
Korea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South KoreaKorea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South Korea
Ahn, Taebin
Kim, Jong Hun
论文数: 0引用数: 0
h-index: 0
机构:
Korea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South KoreaKorea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South Korea
Kim, Jong Hun
Yang, Hee-Man
论文数: 0引用数: 0
h-index: 0
机构:
Korea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South KoreaKorea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South Korea
Yang, Hee-Man
Lee, Jeong Woo
论文数: 0引用数: 0
h-index: 0
机构:
Korea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South KoreaKorea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South Korea
Lee, Jeong Woo
Kim, Jong-Duk
论文数: 0引用数: 0
h-index: 0
机构:
Korea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South Korea
Korea Adv Inst Sci & Technol, Ctr Energy & Environm Engn, Taejon 305701, South KoreaKorea Adv Inst Sci & Technol, Dept Chem & Biomol Engn, Grad Program BK21, Taejon 305701, South Korea
机构:
Cornell Univ, Dept Mat Sci & Engn, Ithaca, NY 14853 USACornell Univ, Dept Mat Sci & Engn, Ithaca, NY 14853 USA
Asenath-Smith, Emily
Estroff, Lara A.
论文数: 0引用数: 0
h-index: 0
机构:
Cornell Univ, Dept Mat Sci & Engn, Ithaca, NY 14853 USA
Cornell Univ, Kavli Inst Cornell Nanoscale Sci, Ithaca, NY 14853 USACornell Univ, Dept Mat Sci & Engn, Ithaca, NY 14853 USA
机构:
Univ New S Wales, Sch Civil & Environm Engn, UNSW Sydney New South Wales, Sydney, NSW 2052, AustraliaUniv New S Wales, Sch Civil & Environm Engn, UNSW Sydney New South Wales, Sydney, NSW 2052, Australia
Boland, Daniel D.
Collins, Richard N.
论文数: 0引用数: 0
h-index: 0
机构:
Univ New S Wales, Sch Civil & Environm Engn, UNSW Sydney New South Wales, Sydney, NSW 2052, AustraliaUniv New S Wales, Sch Civil & Environm Engn, UNSW Sydney New South Wales, Sydney, NSW 2052, Australia
Collins, Richard N.
Miller, Christopher J.
论文数: 0引用数: 0
h-index: 0
机构:
Univ New S Wales, Sch Civil & Environm Engn, UNSW Sydney New South Wales, Sydney, NSW 2052, AustraliaUniv New S Wales, Sch Civil & Environm Engn, UNSW Sydney New South Wales, Sydney, NSW 2052, Australia
Miller, Christopher J.
Glover, Chris J.
论文数: 0引用数: 0
h-index: 0
机构:
Australian Synchrotron, Clayton, Vic 3168, AustraliaUniv New S Wales, Sch Civil & Environm Engn, UNSW Sydney New South Wales, Sydney, NSW 2052, Australia
Glover, Chris J.
Waite, T. David
论文数: 0引用数: 0
h-index: 0
机构:
Univ New S Wales, Sch Civil & Environm Engn, UNSW Sydney New South Wales, Sydney, NSW 2052, AustraliaUniv New S Wales, Sch Civil & Environm Engn, UNSW Sydney New South Wales, Sydney, NSW 2052, Australia
机构:
Tunceli Univ, Fac Engn, Dept Environm Engn, TR-62000 Tunceli, TurkeyTunceli Univ, Fac Engn, Dept Environm Engn, TR-62000 Tunceli, Turkey
Demir, Veysel
Ates, Mehmet
论文数: 0引用数: 0
h-index: 0
机构:
Tunceli Univ, Fac Engn, Dept Bioengn, TR-62000 Tunceli, Turkey
Jackson State Univ, Dept Chem & Biochem, Jackson, MS 39217 USATunceli Univ, Fac Engn, Dept Environm Engn, TR-62000 Tunceli, Turkey
Ates, Mehmet
Arslan, Zikri
论文数: 0引用数: 0
h-index: 0
机构:
Jackson State Univ, Dept Chem & Biochem, Jackson, MS 39217 USATunceli Univ, Fac Engn, Dept Environm Engn, TR-62000 Tunceli, Turkey
Arslan, Zikri
Camas, Mustafa
论文数: 0引用数: 0
h-index: 0
机构:
Tunceli Univ, Fac Engn, Dept Bioengn, TR-62000 Tunceli, TurkeyTunceli Univ, Fac Engn, Dept Environm Engn, TR-62000 Tunceli, Turkey
Camas, Mustafa
Celik, Fatih
论文数: 0引用数: 0
h-index: 0
机构:
Tunceli Univ, Fac Engn, Dept Bioengn, TR-62000 Tunceli, TurkeyTunceli Univ, Fac Engn, Dept Environm Engn, TR-62000 Tunceli, Turkey
Celik, Fatih
Bogatu, Corneliu
论文数: 0引用数: 0
h-index: 0
机构:
Jackson State Univ, Dept Civil & Environm Engn, Jackson, MS 39217 USATunceli Univ, Fac Engn, Dept Environm Engn, TR-62000 Tunceli, Turkey
Bogatu, Corneliu
Can, Safak Seyhaneyildiz
论文数: 0引用数: 0
h-index: 0
机构:
Tunceli Univ, Fac Engn, Dept Bioengn, TR-62000 Tunceli, TurkeyTunceli Univ, Fac Engn, Dept Environm Engn, TR-62000 Tunceli, Turkey
机构:
Univ La Rochelle, CNRS, Littoral Environm Soc, UMR 6250, F-17000 La Rochelle, France
CNRS, FR 3097, F-75700 Paris, FranceUniv La Rochelle, Lab Etude Mat Milieu Agressif, EA3167, F-17042 La Rochelle 01, France
Gilbert, Francoise
Refait, Philippe
论文数: 0引用数: 0
h-index: 0
机构:
Univ La Rochelle, Lab Etude Mat Milieu Agressif, EA3167, F-17042 La Rochelle 01, France
CNRS, FR 3097, F-75700 Paris, FranceUniv La Rochelle, Lab Etude Mat Milieu Agressif, EA3167, F-17042 La Rochelle 01, France
Refait, Philippe
Leveque, Francoiss
论文数: 0引用数: 0
h-index: 0
机构:
Univ La Rochelle, CNRS, Littoral Environm Soc, UMR 6250, F-17000 La Rochelle, France
CNRS, FR 3097, F-75700 Paris, FranceUniv La Rochelle, Lab Etude Mat Milieu Agressif, EA3167, F-17042 La Rochelle 01, France
Leveque, Francoiss
Remazeilles, Celine
论文数: 0引用数: 0
h-index: 0
机构:
Univ La Rochelle, Lab Etude Mat Milieu Agressif, EA3167, F-17042 La Rochelle 01, France
CNRS, FR 3097, F-75700 Paris, FranceUniv La Rochelle, Lab Etude Mat Milieu Agressif, EA3167, F-17042 La Rochelle 01, France
Remazeilles, Celine
Conforto, Egle
论文数: 0引用数: 0
h-index: 0
机构:
Univ La Rochelle, Ctr Commun Analyse, F-17071 La Rochelle 09, France
CNRS, FR 3097, F-75700 Paris, FranceUniv La Rochelle, Lab Etude Mat Milieu Agressif, EA3167, F-17042 La Rochelle 01, France
机构:
Sorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, FranceSorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, France
Guyodo, Yohan
Bonville, Pierre
论文数: 0引用数: 0
h-index: 0
机构:
Univ Paris Saclay, CEA Saclay, Serv Phys Etat Condense, CEA,CNRS, Gif Sur Yvette, FranceSorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, France
Bonville, Pierre
Till, Jessica L.
论文数: 0引用数: 0
h-index: 0
机构:
Sorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, France
Deutsch GeoForsch Zentrum, Potsdam, GermanySorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, France
Till, Jessica L.
Ona-Nguema, Georges
论文数: 0引用数: 0
h-index: 0
机构:
Sorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, FranceSorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, France
Ona-Nguema, Georges
Lagroix, France
论文数: 0引用数: 0
h-index: 0
机构:
Sorbonne Paris Cite, UPD, CNRS UMR 7154, Inst Phys Globe Paris, Paris, FranceSorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, France
Lagroix, France
Menguy, Nicolas
论文数: 0引用数: 0
h-index: 0
机构:
Sorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, FranceSorbonne Univ, UPMC, Inst Mineral Phys Mat & Cosmochim, Museum Natl Hist Nat,Inst Dev UMR 206,CNRS UMR759, Paris, France