Preparation and Characterization of Nanostructured Hydroxyapatite Using a Biomaterial

被引：25
作者：
Neelakandeswari, N. [1 ]
Sangami, G. [1 ]
Dharmaraj, N. [1 ]
机构：
[1] Bharathiar Univ, Dept Chem, Coimbatore 641046, Tamil Nadu, India
来源：
SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY | 2011年 / 41卷 / 05期
关键词：
eggshell membrane; electron microscopy; hydroxyapatite; infrared spectroscopy; x-ray diffraction; SOLID-STATE SYNTHESIS; CATALYST; METAL; EFFICIENT; NICKEL;
D O I：
10.1080/15533174.2011.568434
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Nanostructured needle like, hydroxyapatite (HAp) samples were prepared by a simple approach using biomaterial (egg shell membrane) and characterized by Fourier transform infra-red spectroscopy (FT-IR), powder X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM) techniques. The elemental composition of one of the samples determined by EDAX showed the ratio of Ca/P as 1.425, as expected for the HAp. XRD shows the presence of hexagonal phase for all the samples prepared under various pH conditions. Crystallite size and cell parameters were calculated based on the XRD data.
引用
收藏
页码：513 / 516
页数：4
相关论文
共 35 条
  • [1] Synthesis and characterization of hydroxyapatite using carbon nanotubes as a nano-matrix
    Aryal, S
    Bahadur, KCR
    Dharmaraj, N
    Kim, KW
    Kim, HY
    [J]. SCRIPTA MATERIALIA, 2006, 54 (02) : 131 - 135
  • [2] Synthesis of carbonated hydroxyapatite nanofibers by mechanochemical methods
    Cai, S
    Wang, YW
    Hong, L
    Peng, ZZ
    Yao, KD
    [J]. CERAMICS INTERNATIONAL, 2005, 31 (01) : 135 - 138
  • [3] Microwave-assisted solid-state synthesis of hydroxyapatite nanorods at room temperature
    Cao, JM
    Feng, J
    Deng, SG
    Chang, X
    Wang, J
    Liu, JS
    Lu, P
    Lu, HX
    Zheng, MB
    Zhang, F
    Tao, J
    [J]. JOURNAL OF MATERIALS SCIENCE, 2005, 40 (23) : 6311 - 6313
  • [4] Copper and zinc decontamination from single- and binary-metal solutions using hydroxyapatite
    Corami, Alessia
    Mignardi, Silvano
    Ferrini, Vincenzo
    [J]. JOURNAL OF HAZARDOUS MATERIALS, 2007, 146 (1-2) : 164 - 170
  • [5] Cullity B. D., 1978, ELEMENTS XRAY DIFFRA
  • [6] Metal organic chemical vapour deposition (MOCVD) of bone mineral like carbonated hydroxyapatite coatings
    Darr, JA
    Guo, ZX
    Raman, V
    Bououdina, M
    Rehman, IU
    [J]. CHEMICAL COMMUNICATIONS, 2004, (06) : 696 - 697
  • [7] Dong AG, 2002, ADV MATER, V14, P926, DOI 10.1002/1521-4095(20020618)14:12<926::AID-ADMA926>3.0.CO
  • [8] 2-1
  • [9] Fan Y., 2008, FRONTIERMAT SCI CH, V2, P91, DOI [10.1007/s11706-008-0016-6, DOI 10.1007/S11706-008-0016-6]
  • [10] Effect of reaction temperature on the morphology and size of hydroxyapatite nanoparticles in an emulsion system
    Furuzono, T
    Walsh, D
    Sato, K
    Sonoda, K
    Tanaka, J
    [J]. JOURNAL OF MATERIALS SCIENCE LETTERS, 2001, 20 (02) : 111 - 114
1234