Synthesis, molecular and electronic structure of [ReCl2(N2COPh)(C4N2H4)(PPh3)2]

被引:4
作者
Michalik, S
Dziegielewski, JO
Kruszynski, R
机构
[1] Silesian Univ, Inst Chem, Dept Inorgan & Radiat Chem, PL-40006 Katowice, Poland
[2] Tech Univ Lodz, Inst Gen & Ecol Chem, Xray Crystallog Lab, PL-90924 Lodz, Poland
关键词
rhenium; organodiazenido complexes; X-ray structure;
D O I
10.1080/00958970500239930
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
A new organodiazenido rhenium complex, [ReCl2(N2COPh)(C4N2H4)(PPh3)(2)] has been obtained from the direct reaction of [ReCl2(eta(2)-N2COPh-N',O)(PPh3)(2)] with pyrazine in acetone. The complex has been characterized by spectroscopic methods and its structure determined using single-crystal X-ray diffraction techniques.
引用
收藏
页码:1493 / 1498
页数:6
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