Microwave-assisted synthesis of nanosized Bi2Se3

被引：60

作者：

Harpeness, R ^{[1
]}

Gedanken, A ^{[1
]}

机构：

[1] Bar Ilan Univ, Dept Chem, IL-52900 Ramat Gan, Israel

来源：

NEW JOURNAL OF CHEMISTRY | 2003年 / 27卷 / 08期

关键词：

D O I：

10.1039/b300050h

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The polyol method was applied to the microwave synthesis of nanostructured Bi2Se3. Nanosized Bi particles were obtained as an intermediate in this reaction. The product was characterized by XRD, EDAX, and TEM measurements. The corresponding reaction with tellurium did not yield Bi2Te3. Instead Bi(3)Te(4)is obtained.

引用

收藏

页码：1191 / 1193

页数：3

相关论文

共 28 条

[1]

ATAKULOV SB, 1982, SOV PHYS SEMICOND+, V16, P1326

[2] MICROWAVE-ASSISTED ORGANIC-REACTIONS [J].

CADDICK, S .

TETRAHEDRON, 1995, 51 (38) :10403-10432

[3] An efficient catalyst for asymmetric epoxidation of terminal olefins [J].

Collman, JP ;

Wang, Z ;

Straumanis, A ;

Quelquejeu, M ;

Rose, E .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1999, 121 (02) :460-461

[4]

Desai JD, 1999, B ELECTROCHEM, V15, P315

[5] Influence of spectral diffusion on the line shapes of single CdSe nanocrystallite quantum dots [J].

Empedocles, SA ;

Bawendi, MG .

JOURNAL OF PHYSICAL CHEMISTRY B, 1999, 103 (11) :1826-1830

[6] Rate enhancement of organic reactions by microwaves at atmospheric pressure [J].

Gedye, RN ;

Wei, JB .

CANADIAN JOURNAL OF CHEMISTRY-REVUE CANADIENNE DE CHIMIE, 1998, 76 (05) :525-532

[7] Elaboration of Bi2Se3 by metalorganic chemical vapour deposition [J].

Giani, A ;

Al Bayaz, A ;

Foucaran, A ;

Pascal-Delannoy, F ;

Boyer, A .

JOURNAL OF CRYSTAL GROWTH, 2002, 236 (1-3) :217-220

[8] SOLAR THERMOELECTRIC GENERATION USING BISMUTH TELLURIDE ALLOYS [J].

GOLDSMID, HJ ;

GIUTRONICH, JE ;

KAILA, MM .

SOLAR ENERGY, 1980, 24 (05) :435-440

[9] QUANTUM-SIZE EFFECTS IN THE STUDY OF CHEMICAL SOLUTION DEPOSITION MECHANISMS OF SEMICONDUCTOR-FILMS [J].

GORER, S ;

HODES, G .

JOURNAL OF PHYSICAL CHEMISTRY, 1994, 98 (20) :5338-5346

[10] LIGHT-INDUCED REDOX REACTIONS IN NANOCRYSTALLINE SYSTEMS [J].

HAGFELDT, A ;

GRATZEL, M .

CHEMICAL REVIEWS, 1995, 95 (01) :49-68