Simple adaptation of the Bridgman high pressure technique for use with liquid media

被引:38
作者
Colombier, E. [1 ]
Braithwaite, D. [1 ]
机构
[1] CEA, Dept Rech Fondamentale Matiere Condensee, SPSMS, F-38054 Grenoble, France
关键词
D O I
10.1063/1.2778629
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
We present a simple novel technique to adapt a standard Bridgman cell for the use of a liquid pressure transmitting medium. The technique has been implemented in a compact cell, able to fit in a commercial Quantum Design PPMS system, and would also be easily adaptable to extreme conditions of very low temperatures or high magnetic fields. Several media have been tested and a mix of fluorinert FC84:FC87 has been shown to produce a considerable improvement over the pressure conditions in the standard steatite solid medium, while allowing a relatively easy setup procedure. For optimized hydrostatic conditions, the success rate is about 80% and the maximum pressure achieved so far is 7.1 GPa. Results are shown for the heavy fermion system YbAl3 and for NaV6O15, an insulator showing charge order. (c) 2007 American Institute of Physics.
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页数:5
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