A simple procedure for the synthesis of benzoxanthene derivatives under microwave irradiation conditions

被引:17
作者
Chen, Yan [2 ]
Wu, Shanshan [1 ]
Tu, Shujiang [1 ]
Li, Chunmei [1 ]
Shi, Feng [1 ]
机构
[1] Xuzhou Normal Univ, Sch Chem & Chem Engn, Key Lab Biotechnol Med Plant, Xuzhou 221009, Jiangsu, Peoples R China
[2] Xuzhou Inst Technol Coll, Sch Chem & Chem Engn, Xuzhou 221008, Jiangsu, Peoples R China
关键词
D O I
10.1002/jhet.5570450345
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A rapid and efficient method is developed to synthesize a series of benzoxanthene derivatives by the reaction of aldehydes and 2-hydroxynaphthalene-1,4-dione in mixed solvent of acetic acid and ethylene glycol under microwave irradiation. The method has the advantages of short synthetic route, operational simplicity and higher yields (70%similar to 85%).
引用
收藏
页码:931 / 934
页数:4
相关论文
共 20 条
[1]   Heteropolyacid:: An efficient and eco-friendly catalyst for the synthesis of 14-aryl-14H-dibenzo[a,j]xanthene [J].
Amini, Mostafa Mohammadpour ;
Seyyedhamzeh, Mozhdeh ;
Bazgir, Ayoob .
APPLIED CATALYSIS A-GENERAL, 2007, 323 :242-245
[2]  
Andreani L.L., 1960, BOLL CHIM FARM, V99, P583
[3]   Tetra-methyl ammonium hydroxide:: An efficient and versatile catalyst for the one-pot synthesis of tetrahydrobenzo[b]pyran derivatives in aqueous media [J].
Balalaie, Saeed ;
Sheikh-Ahmadi, Masoumeh ;
Bararjanian, Morteza .
CATALYSIS COMMUNICATIONS, 2007, 8 (11) :1724-1728
[4]   CHEMICAL ASPECTS OF SANTALIN AS A HISTOLOGICAL STAIN [J].
BANERJEE, A ;
MUKHERJEE, AK .
STAIN TECHNOLOGY, 1981, 56 (02) :83-85
[5]  
BONSIGNRE L, 1983, EUR J MED CHEM, V28, P517
[6]  
Grieco P.A., 1998, Organic Synthesis in Water, DOI [10.1007/978-94-011-4950-1, DOI 10.1007/978-94-011-4950-1]
[7]  
Hideo T., 1981, Jpn Tokkyo Koho, Patent No. [JP56005480, 56005480, JP 56 005 480]
[8]  
Kappe CO, 2005, METH PRIN MED CHEM, V52, P1, DOI 10.1002/3527606556
[9]  
KAPPE CO, 2005, ANGEW CHEM COMMUN, P2881
[10]  
Khoramabadi-zad A, 2005, J CHEM RES, P277