Effect of MgO-TiO2-SiO2 additions on in-situ anisotropic grains growth and mechanical properties of corundum abrasive using pseudo-boehmite as raw material

被引:12
作者
Han, Yang [1 ]
Li, Zhihong [1 ]
Zhu, Yumei [1 ]
机构
[1] Tianjin Univ, Sch Mat Sci & Engn, Key Lab Adv Ceram & Machining Technol, Minist Educ, Tianjin 300072, Peoples R China
关键词
Pseudo-boehmite; Microcrystalline corundum abrasives; Anisotropic grains; Sol-gel processes; Fracture toughness; FRACTURE-TOUGHNESS; ALUMINA CERAMICS; MGO; MICROSTRUCTURE; BEHAVIOR; WEAR; SIO2;
D O I
10.1016/j.ceramint.2019.09.171
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Microcrystalline corundum abrasives with a duplex microstructure consisting of elongated anisotropic grains and fine equiaxed grains were fabricated via sol-gel processes using pseudo-boehmite as raw material. Elongated anisotropic grain, as a second phase reinforcement, significantly improved the fracture toughness and strength of samples. When the sample was doped 2 wt% MgO-TiO2-SiO2 additions with the molar ratio of 3:5:11, elongated anisotropic grains had the highest aspect ratio and were uniformly distributed among the fine equiaxed grains matrix. In addition, the sample obtained a maximum density above 3.92 g cm(-3), single particle compressive strength of 56.4 N and fracture toughness of 5.93 MPa m(1/2). The relationship between the microstructure and the mechanical properties of the abrasives was also discussed in detail. Moreover, toughening mechanism of elongated anisotropic grains was clearly explained by charactering crack propagation and fracture surfaces of samples.
引用
收藏
页码:1934 / 1939
页数:6
相关论文
共 27 条
  • [1] A CRITICAL-EVALUATION OF INDENTATION TECHNIQUES FOR MEASURING FRACTURE-TOUGHNESS .1. DIRECT CRACK MEASUREMENTS
    ANSTIS, GR
    CHANTIKUL, P
    LAWN, BR
    MARSHALL, DB
    [J]. JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1981, 64 (09) : 533 - 538
  • [2] Bae IJ, 1997, J AM CERAM SOC, V80, P1149
  • [3] CRITICAL CONCENTRATION OF MGO FOR THE PREVENTION OF ABNORMAL GRAIN-GROWTH IN ALUMINA
    BAE, SI
    BAIK, S
    [J]. JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1994, 77 (10) : 2499 - 2504
  • [4] Microstructural coarsening of zirconia-toughened alumina composites
    Casellas, D
    Nagl, MM
    Llanes, L
    Anglada, M
    [J]. JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2005, 88 (07) : 1958 - 1963
  • [5] Chemical inhomogeneity in commercial alumina powders and its effect on abnormal grain growth during sintering
    Cho, SJ
    Lee, YC
    Lee, HL
    Sim, SM
    Yanagisawa, M
    [J]. JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 2003, 23 (13) : 2281 - 2288
  • [6] Collin MIK, 2001, J AM CERAM SOC, V84, P1334, DOI 10.1111/j.1151-2916.2001.tb00838.x
  • [7] Effects of silicon carbide nano-phase on the wet erosive wear of polycrystalline alumina
    Davidge, RW
    Twigg, PC
    Riley, FL
    [J]. JOURNAL OF THE EUROPEAN CERAMIC SOCIETY, 1996, 16 (07) : 799 - 802
  • [8] Influence of whisker toughening and microstructure on the wear behavior of Si3N4- and Al2O3-matrix composites reinforced with SiC
    Dogan, CP
    Hawk, JA
    [J]. JOURNAL OF MATERIALS SCIENCE, 2000, 35 (23) : 5793 - 5807
  • [9] Synthesis and properties of porous alumina ceramics with inter-locked plate-like structure through the tert-butyl alcohol-based gel-casting method
    Dong, Xue
    Wang, Mingchao
    Guo, Anran
    Zhang, Yongxin
    Ren, Sue
    Sui, Guofa
    Du, Haiyan
    [J]. JOURNAL OF ALLOYS AND COMPOUNDS, 2017, 694 : 1045 - 1053
  • [10] Effect of ZnF2-TiO2-SiO2 additions on the two-step sintering behavior and mechanical properties of sol-gel derived corundum abrasive
    Hu, Dezhi
    Li, Zhihong
    Zhu, Yumei
    [J]. CERAMICS INTERNATIONAL, 2016, 42 (06) : 7373 - 7379