2-hydroxy-3-methoxybenzaldehyde 2,4-dinitrophenylhydrazone dimethylformamide solvate

被引:12
作者
Jing, ZL [1 ]
Yu, M [1 ]
Chen, X [1 ]
Diao, CH [1 ]
Deng, QL [1 ]
Fan, Z [1 ]
机构
[1] Tianjin Univ Sci & Technol, Coll Sci, Tianjin 300222, Peoples R China
关键词
D O I
10.1107/S1600536804032878
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C14H12N4O6 . C3H7NO, was prepared by the reaction of 2-hydroxy-3-methoxybenzaldehyde and 2,4-dinitrophenylhydrazine in N,N-dimethylformamide. In the crystal structure, the molecule of 2-hydroxy-3-methoxybenzaldehyde-2,4- dinitrophenylhydrazone is approximately planar, with a mean deviation of non-H atoms from the plane of 0.109 Angstrom. The crystal packing is stabilized by O - H ... O and N - H ... O hydrogen bonds and aromatic packing interactions.
引用
收藏
页码:O145 / O146
页数:2
相关论文
共 6 条
[1]  
*BRUK AXS INC, 1999, SADABS SHELXTL SMART
[2]  
Farrugia L. J., 1999, J. Appl. Crystallogr, V32, P837, DOI DOI 10.1107/S0021889899006020
[3]   Structure and spectroscopic characteristics of N,N′-bis (2-hydroxy-3-methoxyphenylmethylidene)-2,6-pyridinediamine [J].
Galic, N ;
Matkovic-Calogovic, D ;
Cimerman, Z .
STRUCTURAL CHEMISTRY, 2000, 11 (06) :361-365
[4]  
HE RX, 2002, CHEM J CHINESE U, V23, P991
[5]  
LI SL, 1995, CHINESE J STRUC CHEM, V14, P88
[6]  
Sheldrick G. M., 1997, SHELXS 97 PROGRAM CR