7-Fluoroisatin-1,4-dioxane(1/1)

被引：11
作者：
Shankland, Kenneth
Leech, Charlotte K.
Mohamed, Sharmarke
Barnett, Sarah A.
Tocher, Derek A.
机构：
[1] UCL, Dept Chem, London WC1H 0AJ, England
[2] Rutherford Appleton Lab, ISIS Facil, Didcot OX11 0QX, Oxon, England
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2007年 / 63卷
关键词：
D O I：
10.1107/S1600536807035258
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title 1,4-dioxane solvate, C (8)H(4)FNO(2)center dot C(4)H(8)O(2), was isolated during a manual crystallization screen on 7-fluoroisatin (7-fluoroindoline-2,3-dione). The 7-fluoroisatin molecule occupies a general position and each of the independent molecules of 1,4-dioxane is disposed about a centre of inversion, with half of each in the asymmetric unit. Hydrogen-bonded ribbons of 7-fluoroisatin are linked by 1,4-dioxane to form sheets parallel to (30 (1) over bar). Whilst one solvent molecule has an active role in the sheet formation, the other simply fills the cavity formed within the sheet.
引用
收藏
页码：O3574 / U4110
页数：10
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