X-ray powder diffraction data for 2-[((3R)-5-oxo-4-phenyltetrahy drofuran-3-yl)methyl]isoindoline-1,3-dione, C19H15NO4

被引：1

作者：

Zheng, Shoujun ^{[1
]}

Xu, Kailin ^{[1
]}

Wang, Qing ^{[1
]}

Tang, XiaoLin ^{[2
]}

Huang, Yanmei ^{[1
]}

Tang, Pei Xiao ^{[1
]}

Chen, Lijuan ^{[1
]}

Li, Hui ^{[1
]}

机构：

[1] Sichuan Univ, Coll Chem Engn, Chengdu 610065, Peoples R China

[2] Sichuan CheCO Pharmaceut Technol Co Ltd, Chengdu 610041, Peoples R China

来源：

POWDER DIFFRACTION | 2016年 / 31卷 / 02期

关键词：

X-ray powder diffraction; 2-[((3R)-5-oxo-4-phenyltetrahy drofuran-3-yl)methyl]isoindoline-1,3-dione; Milnacipran hydrochloride; RELIABILITY; CRITERION; PATTERNS;

D O I：

10.1017/S0885715616000105

中图分类号：

TB3 [工程材料学];

学科分类号：

0805 ; 080502 ;

摘要：

2-[((3R)-5-oxo-4-phenyltetrahydrofuran-3-yl)methyl]isoindoline-1,3-dione, C19H15NO4, was synthesized for the first time. Its structure was characterized by element analysis, ultraviolet spectrometry, nuclear magnetic resonance, and single X-ray diffraction (SXRD). X-ray powder diffraction (XRPD) data of title compound were collected and calculated. The result of SXRD shows that its crystal system is orthorhombic, space group is Pbca, and unit-cell parameters are a = 8.861 57(7), b = 14.6666(10), c = 24.4247(19) angstrom, alpha=beta=gamma=90 degrees, unit-cell volume V = 3174.4 angstrom(3), and Z = 8. All XRPD measured lines were indexed and consistent with the Pbca space group [a = 14.639(7), b = 24.378(3), c = 8.918(1) angstrom, alpha=beta=gamma=90 degrees, unit-cell volume V = 3182.7(9) angstrom(3), Z = 8]. No detectable impurities were observed. (C) 2016 International Centre for Diffraction Data.

引用

页码：155 / 158

页数：4

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