Possibilities of low-level determination of silicon in biological materials by activation analysis

被引:7
作者
Kucera, J [1 ]
Randa, Z [1 ]
机构
[1] Acad Sci Czech Republ, Inst Nucl Phys, CZ-25068 Rez, Czech Republic
来源
FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY | 2001年 / 370卷 / 2-3期
关键词
D O I
10.1007/s002160100802
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The capabilities of neutron and photon activation analysis (NAA and PAA, respectively) for low-level determination of silicon in biological materials have been examined. Sensitivities of a variety of modes of NAA and PAA with radiochemical separation have been evaluated. Results are presented for silicon in reference materials CSRM 12-2-03 Lucerne, Bowen's Kale, NIST SRM-1571 Orchard Leaves, and NIST SRM-1515 Apple Leaves. The results were obtained by employing the Si-29(n,p)Al-29 reaction with fast reactor neutrons and the radiochemical procedure developed for aluminium separation. Possibilities of further improvement of the silicon determination limit down to the mug g(-1) level by employing NAA and PAA with radiochemical separation are outlined.
引用
收藏
页码:241 / 245
页数:5
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