Phase Separation in Aged Diffusion-Couples Fe/Fe-40 at%Cr Alloy

被引:0
作者
Lopez-Hirata, Victor M. [1 ]
Cayetano-Castro, Nicolas [1 ]
Dorantes-Rosales, Hector J. [1 ]
Saucedo-Munoz, Maribel L. [1 ]
Avila-Davila, Erika O. [2 ]
机构
[1] Inst Politecn Nacl ESIQIE, Mexico City 07051, DF, Mexico
[2] Inst Tecnol Pachuca, Pachuca De Soto Hgo 42080, Mexico
关键词
iron-chromium alloys; phase separation; diffusion-couple; aging; hardening; SPINODAL DECOMPOSITION;
D O I
10.2320/matertrans.M2011230
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Diffusion-couples of pure Fe/Fe-40 at%Cr alloy were used to analyze the phase separation process in Fe-Cr alloys. Diffusion-couples were solution treated at 1050 degrees C for 3.6 ks and subsequently aged at 500 degrees C for 3.6-3600 ks. Interdiffusion zones were analyzed by HR-TEM and hardness measurements. The EDS-SEM analysis of solution treated, water-quenched and then aged diffusion-couple permitted to obtain the equilibrium composition of miscibility gap at 500 degrees C to be 14 at% Cr. The HR-TEM analysis of the aged diffusion-couple showed the change in size and volume percentages of precipitates with composition. The hardness measurements of the aged diffusion-couple indicated the age hardening due to the presence of nanometric Cr-rich precipitates in a Fe-rich matrix. [doi:10.2320/matertrans.M2011230]
引用
收藏
页码:2155 / 2158
页数:4
相关论文
共 11 条
  • [1] SPINODAL DECOMPOSITION OF IRON-32 AT -PERCENT CHROMIUM AT 470-DEGREES-C
    BRENNER, SS
    MILLER, MK
    SOFFA, WA
    [J]. SCRIPTA METALLURGICA, 1982, 16 (07): : 831 - 836
  • [2] SPINODAL DECOMPOSITION - REPRISE
    CAHN, JW
    HILLIARD, JE
    [J]. ACTA METALLURGICA, 1971, 19 (02): : 151 - +
  • [3] Atom probe studies of the Fe-Cr system and stainless steels aged at intermediate temperature: A review
    Danoix, F
    Auger, P
    [J]. MATERIALS CHARACTERIZATION, 2000, 44 (1-2) : 177 - 201
  • [4] Gibbs-Thomson relationship for the precipitation in Cu-Ti alloys
    Hemandez-Santiago, Felipe
    Lopez-Hirata, Victor M.
    Saucedo-Munoz, Manbel L.
    Dorantes-Rosales, Hector J.
    [J]. MATERIALS CHARACTERIZATION, 2007, 58 (03) : 303 - 306
  • [5] FURTHER-STUDIES OF SPINODAL DECOMPOSITION IN FE-CR
    LASALLE, JC
    SCHWARTZ, LH
    [J]. ACTA METALLURGICA, 1986, 34 (06): : 989 - 1000
  • [6] Marshal P., 1990, AUSTENITIC STAINLESS, P1
  • [7] SPINODAL DECOMPOSITION IN FE-CR ALLOYS - EXPERIMENTAL-STUDY AT THE ATOMIC-LEVEL AND COMPARISON WITH COMPUTER-MODELS .1. INTRODUCTION AND METHODOLOGY
    MILLER, MK
    HYDE, JM
    HETHERINGTON, MG
    CEREZO, A
    SMITH, GDW
    ELLIOTT, CM
    [J]. ACTA METALLURGICA ET MATERIALIA, 1995, 43 (09): : 3385 - 3401
  • [8] A new characterization method of the microstructure using the macroscopic composition gradient in alloys
    Miyazaki, T
    Koyama, T
    Kobayashi, S
    [J]. METALLURGICAL AND MATERIALS TRANSACTIONS A-PHYSICAL METALLURGY AND MATERIALS SCIENCE, 1996, 27 (04): : 945 - 949
  • [9] Effect of 475 °C embrittlement on the mechanical properties of duplex stainless steel
    Sahu, J. K.
    Krupp, U.
    Ghosh, R. N.
    Christ, H. -J.
    [J]. MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2009, 508 (1-2): : 1 - 14
  • [10] Effect of spinodal decomposition on the mechanical behavior of Fe-Cr alloys
    Soriano-Vargas, Orlando
    Avila-Davila, Erika O.
    Lopez-Hirata, Victor M.
    Cayetano-Castro, Nicolas
    Gonzalez-Velazquez, Jorge L.
    [J]. MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2010, 527 (12): : 2910 - 2914