Morphology control and optical characterization of three-dimensional ordered macroporous Cu films from template-assisted electrodeposition

被引:3
作者
Meng, Xiangdong [1 ]
Song, Yang [1 ]
Shu, Ting [2 ]
机构
[1] Jilin Normal Univ, Key Lab Funct Mat Phys & Chem, Minist Educ, Changchun 130023, Jilin, Peoples R China
[2] Hubei Univ Sci & Technol, Xianning 437100, Hubei, Peoples R China
关键词
Three-dimensional ordered macroporous; Polystyrene templates; Cu films; Electrodeposition parameters; Electrodeposition method; POROUS COPPER-FILMS; PERFORMANCE; FABRICATION; CARBON;
D O I
10.1007/s10934-020-00883-3
中图分类号
O69 [应用化学];
学科分类号
081704 ;
摘要
Three-dimensional ordered macroporous (3DOM) Cu films with the size 300-500 nm were prepared on FTO by colloidal crystal template-assisted electrodeposition in aqueous solution. The effects of electrodeposition methods and electrodeposition parameters on the morphology and structure of the 3DOM copper films were studied. It is found that the constant potential method is more suitable for the preparation of 3DOM copper films compared to the step electrodeposition method, the deposition voltage affects the grain size and the flatness of the copper film surface and the electrodeposition time affects the dimension and the number of layers of the copper films. The optical properties of the prepared 3DOM copper films were also analyzed.
引用
收藏
页码:1069 / 1076
页数:8
相关论文
共 23 条
  • [11] 3D Porous Copper Films with Large Specific Surface Prepared by Hydrogen Bubble Template
    Luo, Binbin
    Li, Xueming
    Li, Xianli
    Feng, Wenlin
    [J]. ASIAN JOURNAL OF CHEMISTRY, 2013, 25 (17) : 9927 - 9930
  • [12] Niu JC, 2015, INT J ELECTROCHEM SC, V10, P7331
  • [13] Construction of a 3D porous network of copper film via a template-free deposition method with superior mechanical and electrical properties for micro-energy devices
    Peng, Yuncheng
    Wang, Yao
    Deng, Yuan
    [J]. MATERIALS RESEARCH EXPRESS, 2016, 3 (08):
  • [14] Three-dimensional macroporous Cu electrode: Preparation and electrocatalytic activity for nonenzymatic glucose detection
    Qi, Bin
    Yang, Haijing
    Zhao, Kaiyue
    Bah, Mohamed M.
    Bo, Xiangjie
    Guo, Liping
    [J]. JOURNAL OF ELECTROANALYTICAL CHEMISTRY, 2013, 700 : 24 - 29
  • [15] [孙雅峰 Sun Yafeng], 2006, [电化学, Electrochemistry], V12, P177
  • [16] Pseudocapacitive effect and Li+ diffusion coefficient in three-dimensionally ordered macroporous vanadium oxide for energy storage
    Tong, Zhongqiu
    Xu, Hongbo
    Liu, Guangqun
    Zhao, Jiupeng
    Li, Yao
    [J]. ELECTROCHEMISTRY COMMUNICATIONS, 2016, 69 : 46 - 49
  • [17] Morphologies and wetting properties of copper film with 3D porous micro-nano hierarchical structure prepared by electrochemical deposition
    Wang, Hongbin
    Wang, Ning
    Hang, Tao
    Li, Ming
    [J]. APPLIED SURFACE SCIENCE, 2016, 372 : 7 - 12
  • [18] Preparation of a Novel Form of Gelatin With a Three-Dimensional Ordered Macroporous Structure to Regulate the Release of Poorly Water-Soluble Drugs
    Xu, Jie
    Zhao, Zongzhe
    Hao, Yanna
    Zhao, Ying
    Qiu, Yang
    Jiang, Jie
    Yu, Tong
    Ji, Peng
    Liu, Ying
    Wu, Chao
    [J]. JOURNAL OF PHARMACEUTICAL SCIENCES, 2016, 105 (09) : 2940 - 2948
  • [19] In Situ Electrochemical Fabrication of Three Dimensional Hierarchical Nanoporous Copper Films and Their Electrocatalytic Performance
    Yang, C.
    Zhang, Q. B.
    Gao, M. Y.
    Hua, Y. X.
    Xu, C. Y.
    [J]. JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 2016, 163 (09) : D469 - D475
  • [20] Highly Porous Copper with Hollow Microsphere Structure from Polystyrene Templates via Electroless Plating
    Yu, Qingxia
    Li, Mingyu
    Zeng, Qingxuan
    Wu, Xingyu
    [J]. JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 2017, 164 (04) : D135 - D142