Novel antibacterial cellulose acetate fibers modified with 2-fluoropyridine complexes

被引:16
作者
Demirdogen, Ruken Esra [1 ]
Kilic, Derya [2 ]
Emen, Fatih Mehmet [2 ]
Askar, Sinasi [3 ]
Karacolak, Ali Ihsan [2 ]
Yesilkaynak, Tuncay [4 ]
Ihsan, Ayesha [5 ]
机构
[1] Cankiri Karatekin Univ, Fac Sci, Dept Chem, TR-18100 Cankiri, Turkey
[2] Burdur Mehmet Akif Ersoy Univ, Fac Arts & Sci, Dept Chem, TR-15030 Burdur, Turkey
[3] Cankiri Karatekin Univ, Fac Hlth Sci, Dept Nutr & Dietet, TR-18200 Cankiri, Turkey
[4] Sutcu Imam Univ, Afsin Vocat Sch, Dept Chem Technol, TR-46500 Kahramanmaras, Turkey
[5] Natl Inst Biotechnol & Genet Engn, Nanobiotech Grp, POB 577, Faisalabad, Pakistan
关键词
Electrospinning; Pyridine complexes; Antibacterial textile; Antimicrobial resistance; E; coli; Staphylococcus aureus; SUBSTITUTED-PYRIDINE COMPLEXES; THERMAL-DECOMPOSITION; METAL-COMPLEXES; COPPER; CELLS; THIOSEMICARBAZONES; RESISTANCE; TOXICITY; GALLIUM;
D O I
10.1016/j.molstruc.2019.127537
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
The complexes represented with the general formula [ML2Cl2] (L: 2-fluoropyridine; M: Ni (II), Cu (II), Co (II)) were synthesized and their structures were characterized via FT-IR and H-1 NMR techniques. Thermal properties of the complexes were also investigated via TG/DTA combined system under N-2 atmosphere. The complexes containing cellulose acetate (CA) micro/nano-fibers, which is a biocompatible and biodegradable polymer, were obtained via electrospinning technique. The fibers were characterized via FT-IR spectroscopy. FE-SEM images of the fibers were used to investigate their morphologies and for to determine the diameters of the fibers. Thermal properties of the fibers were investigated via TG/DTA combined system. Antibacterial studies of the complexes and fibers were investigated against the bacteria strains E. coli and Methyciline Resistant Staphylocaucus aureus via disc diffusion, broth microdilution and JIS L 1902: 2008, Testing method for antibacterial activity of textiles. Different levels Antibacterial activity was observed for all complexes and fibers. (C) 2019 Elsevier B.V. All rights reserved.
引用
收藏
页数:8
相关论文
共 42 条
[1]  
Abbott I, 2013, EXPERT REV ANTI-INFE, V11, P395, DOI [10.1586/ERI.13.21, 10.1586/eri.13.21]
[2]   THERMAL DECOMPOSITION OF METAL COMPLEXES .4. PREPARATION AND THERMAL DECOMPOSITION OF SOME PYRIDINE AND SUBSTITUTED-PYRIDINE COMPLEXES OF NUCKEL (2) HALIDES [J].
ALLAN, JR ;
BROWN, DH ;
NUTTALL, RH ;
SHARP, DWA .
JOURNAL OF INORGANIC & NUCLEAR CHEMISTRY, 1965, 27 (07) :1529-&
[3]   THE THERMAL DECOMPOSITION OF METAL COMPLEXES .3. THE DECOMPOSITION OF SOME PYRIDINE AND SUBSTITUTED-PYRIDINE COMPLEXES OF COBALT(II) HALIDES [J].
ALLAN, JR ;
BROWN, DH ;
NUTTALL, RH ;
SHARP, DWA .
JOURNAL OF INORGANIC & NUCLEAR CHEMISTRY, 1964, 26 (11) :1895-1902
[4]  
[Anonymous], 2012, CLSI document M02-A11
[5]  
[Anonymous], L19022008 JIS
[6]  
[Anonymous], INT J SCI
[7]   The potential of desferrioxamine-gallium as an anti-Pseudomonas therapeutic agent [J].
Banin, Ehud ;
Lozinski, Alina ;
Brady, Keith M. ;
Berenshtein, Eduard ;
Butterfield, Phillip W. ;
Moshe, Maya ;
Chevion, Mordechai ;
Greenberg, Everett Peter ;
Banin, Eyal .
PROCEEDINGS OF THE NATIONAL ACADEMY OF SCIENCES OF THE UNITED STATES OF AMERICA, 2008, 105 (43) :16761-16766
[8]   Trifluoromethyl-containing pyrazolinyl (p-tolyl) sulfones:: The synthesis and structure of promising antimicrobial agents [J].
Bonacorso, Helio G. ;
Wentz, Alexandre P. ;
Lourega, Rogerio V. ;
Cechinel, Cleber A. ;
Moraes, Tatiana S. ;
Coelho, Helena S. ;
Zanatta, Nilo ;
Martins, Marcos A. P. ;
Hoerner, Manfredo ;
Alves, Sydney H. .
JOURNAL OF FLUORINE CHEMISTRY, 2006, 127 (08) :1066-1072
[9]  
CLSI-Clinical and Laboratory Standards Institute, 2012, CLSI DOCUMENT M07 A9
[10]  
Codjoe Francis S, 2017, Med Sci (Basel), V6, DOI 10.3390/medsci6010001