Delivery of stable ultra-thin liquid sheets in vacuum for biochemical spectroscopy

被引：17

作者：

Barnard, Jonathan C. T. ^{[1
]}

Lee, Jacob P. ^{[1
]}

Alexander, Oliver ^{[1
]}

Jarosch, Sebastian ^{[1
]}

Garratt, Douglas ^{[1
]}

Picciuto, Rose ^{[1
]}

Kowalczyk, Katarzyna ^{[1
]}

Ferchaud, Clement ^{[1
]}

Gregory, Andrew ^{[1
]}

Matthews, Mary ^{[1
]}

Marangos, Jon P. ^{[1
]}

机构：

[1] Imperial Coll London, Dept Phys, Blackett Lab, Extreme Light Consortium, London, England

来源：

FRONTIERS IN MOLECULAR BIOSCIENCES | 2022年 / 9卷

基金：

英国工程与自然科学研究理事会;

关键词：

XUV spectroscopy; spectroscopy in liquids; microfluidics; liquids in vacuum; interferometry; liquid flatjet; DYNAMICS; FLUID; WATER;

D O I：

10.3389/fmolb.2022.1044610

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

The development of ultra-thin flat liquid sheets capable of running in vacuum has provided an exciting new target for X-ray absorption spectroscopy in the liquid and solution phases. Several methods have become available for delivering in-vacuum sheet jets using different nozzle designs. We compare the sheets produced by two different types of nozzle; a commercially available borosillicate glass chip using microfluidic channels to deliver colliding jets, and an in-house fabricated fan spray nozzle which compresses the liquid on an axis out of a slit to achieve collision conditions. We find in our tests that both nozzles are suitable for use in X-ray absorption spectroscopy with the fan spray nozzle producing thicker but more stable jets than the commercial nozzle. We also provide practical details of how to run these nozzles in vacuum.

引用

页数：9

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