Synthesis and characterization of new thiadiazole derivatives bearing a pyrazole moiety

被引：3

作者：

Sacmaci, Mustafa ^{[1
]}

Arslaner, Ciler ^{[1
]}

Sahin, Ertan ^{[2
]}

机构：

[1] Bozok Univ, Fac Arts & Sci, Dept Chem, Yozgat, Turkey

[2] Ataturk Univ, Fac Sci, Dept Chem, Erzurum, Turkey

来源：

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2017年 / 192卷 / 10期

关键词：

Thiadiazole; pyrazole; X-ray structure; ACID;

D O I：

10.1080/10426507.2017.1345905

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A series of thidiazole derivatives (4, 7) from pyrazole-3-carboxylic acid chloride (2) and pyrazole-3,4-dicarboxylicacid chloride derivatives (6) were synthesized and characterized. The structures of the new compounds were confirmed byelemental analysis, NMR (H-1 and C-13) and IR spectra. The molecular and crystal structure of 4-benzoyl-N-[5-(methylthio)-1,3,4-thiadiazol-2-yl]-1,5-di-phenyl-1H-pyrazole-3carboxamide(4d)was determined by single crystal X-ray diffraction method.

引用

页码：1134 / 1139

页数：6

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