(1R*,5S*)-8-(2-Fluoro-4-nitrophenyl)-8-azabicyclo[3.2.1]octan-3-one

被引：0
|
作者：
Yang, Tao [1 ]
Yang, Jianzhong [1 ]
Li, Zicheng [2 ]
Luo, Youfu [1 ]
机构：
[1] Sichuan Univ, W China Hosp, State Key Lab Biotherapy, Chengdu 610041, Peoples R China
[2] Sichuan Univ, Sch Chem Engn, Dept Pharmaceut & Bioengn, Chengdu 610065, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷
关键词：
data-to-parameter ratio = 11.5; disorder in main residue; mean σ(C-C) = 0.003 Å; R factor = 0.044; single-crystal X-ray study; T = 293 K; wR factor = 0.113;
D O I：
10.1107/S1600536811047350
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C13H13FN2O3, the fused piperidine ring is in a chair conformation. The fused pyrrolidine ring shows an envelope conformation with the N atom displaced by 0.661 (3) angstrom out of the plane formed by the four C atoms of the pyrrolidine ring. The dihedral angle between this plane and the plane formed by the four attached C atoms of the piperidine ring (not including the carbonyl C atom) is 67.63 (10)degrees. The F atom is disordered and was refined using a split model with an occupancy ratio of 0.910 (3): 0.080 (3).
引用
收藏
页码：O3297 / U1809
页数：8
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