Using GISAXS to Detect Correlations between the Locations of Gold Particles Electrodeposited from an Aqueous Solution

被引：10

作者：

Moehl, Gilles E. ^{[1
]}

Bartlett, Philip N. ^{[1
]}

Hector, Andrew L. ^{[1
]}

机构：

[1] Univ Southampton, Sch Chem, Southampton SO17 1BJ, Hants, England

来源：

LANGMUIR | 2020年 / 36卷 / 16期

基金：

英国工程与自然科学研究理事会;

关键词：

SIZE-SELECTIVE ELECTRODEPOSITION; MESOSCALE METAL PARTICLES; IN-SITU; ELECTROCHEMICAL NUCLEATION; X-RAY; SPUTTER-DEPOSITION; SPRAY DEPOSITION; NANOPARTICLES; GROWTH; CARBON;

D O I：

10.1021/acs.langmuir.9b03400

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Electrodeposition is a powerful tool for the bottom-up fabrication of novel electronic devices. This necessitates a complete understanding of the deposition process beyond the classical description using current transients. Recent calculations predict deviations within the spatial arrangement of electrodeposited particles, away from random nucleation. The spatial arrangement of Au particles generated through aqueous electrodeposition on a nontemplated substrate is investigated by grazing incidence small-angle X-ray scattering (GISAXS). We show that GISAXS is able to reveal spatial correlations within deposited particles that are not easily detectable by microscopy.

引用

页码：4432 / 4438

页数：7

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