Synthesis and Crystal Structure of 1,3-Bis[2-(pyrrol-2-carbonyloxy)ethoxy]Benzene

被引：2

作者：

Sun, Shipeng ^{[1
]}

Dong, Li ^{[1
]}

Guo, Jianhua ^{[1
]}

Yin, Zhenming ^{[1
]}

机构：

[1] Tianjin Normal Uinvers, Coll Chem, Tianjin Key Lab Struct & Performance Funct Mol, Tianjin 300387, Peoples R China

来源：

JOURNAL OF CHEMICAL CRYSTALLOGRAPHY | 2010年 / 40卷 / 12期

关键词：

1,3-Bis[2-(pyrrol-2-carbonyloxy)ethoxy]benzene; Synthesis; Crystal structure; Hydrogen bonding motif; BINDING; RECEPTOR; MONOSACCHARIDES; DIMER;

D O I：

10.1007/s10870-010-9810-y

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

A new compound, 1,3-bis[2-(pyrrol-2-carbonyloxy)ethoxy]benzene (1), was synthesized and characterized by X-ray diffraction. The crystal is monoclinic, space group P2(1)/c with a = 6.3571(7), b = 11.0416(11), c = 28.156(3) angstrom, b = 92.821(2), V = 1974.0(4) angstrom(3), Z = 4, Dc = 1.293 g/cm(3), F(000) = 808, mu = 0.097 mm(-1). The final R = 0.0395 and wR = 0.0927 for 3478 observed reflections with I > 2 sigma(I), and R = 0.0660 and wR = 0.1058 for all reflections. The title compound assembles into 2-D structure through a catemer type N-H...O hydrogen bonding motif and further forms 3-D structure through C-H center dot center dot center dot O hydrogen bonds.

引用

页码：1142 / 1145

页数：4

共 30 条

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