An investigation of the inclusion complex of β-cyclodextrin with p-nitrobenzoic acid in the solid state

被引：8

作者：

Fan, Zhi ^{[1
]}

Diao, Chun-Hua ^{[1
]}

Guo, Min-Jie ^{[1
]}

Du, Rong-Juan ^{[1
]}

Song, Yuan-Fang ^{[1
]}

Jing, Zuo-Liang ^{[1
]}

Yu, Ming ^{[1
]}

机构：

[1] Univ Sci & Technol, Coll Sci, Tianjin 300222, Peoples R China

来源：

CARBOHYDRATE RESEARCH | 2007年 / 342卷 / 16期

关键词：

beta-cyclodextrinl; cyclomaltoheptaose inclusion complex; crystal structure; p-nitrobenzoic acid;

D O I：

10.1016/j.carres.2007.07.004

中图分类号：

Q5 [生物化学]; Q7 [分子生物学];

学科分类号：

071010 ; 081704 ;

摘要：

The weak inclusion complex of cyclomaltoheptaose (beta-cyclodextrin, beta CD) with p-nitrobenzoic acid was investigated in the solid state. Crystallography shows that two beta CD molecules co-crystallize with two p-nitrobenzoic acids and 28.5 water molecules [2(C(42)H(70)O(35))center dot 2(C(7)H(5)NO(4))center dot 28 center dot 5H(2)O] in the triclinic system. (C) 2007 Elsevier Ltd. All rights reserved.

引用

页码：2500 / 2503

页数：4

共 18 条

[1] The molecular structure and crystal organization of rac-terfenadine/β-cyclodextrin/tartaric acid multicomponent inclusion complex [J].

Bacchi, A ;

Pelizzi, G ;

Sheldrick, GM ;

Amari, G ;

Delcanale, M ;

Redenti, E .

SUPRAMOLECULAR CHEMISTRY, 2002, 14 (01) :67-74

[2]

BRETT TJ, 2000, J CHEM SOC P2, P1105

[3]

BRETT TJ, 2000, J CHEM SOC P2, P1095

[4] Preparation, thermal behaviour and solid-state structures of inclusion complexes of permethylated-β-cyclodextrin with the garlic-derived antithrombotics (E)- and (Z)-ajoene [J].

Caira, MR ;

Hunter, R ;

Bourne, SA ;

Smith, VJ .

SUPRAMOLECULAR CHEMISTRY, 2004, 16 (06) :395-403

[5] SYNTHESIS AND X-RAY CRYSTAL-STRUCTURE OF BETA-CYCLODEXTRIN DICLOFENAC SODIUM UNDECAHYDRATE, A BETA-CD COMPLEX WITH A UNIQUE CRYSTAL PACKING ARRANGEMENT [J].

CAIRA, MR ;

GRIFFITH, VJ ;

NASSIMBENI, LR ;

VANOUDTSHOORN, B .

JOURNAL OF THE CHEMICAL SOCIETY-CHEMICAL COMMUNICATIONS, 1994, (09) :1061-1062

[6] Crystal structure investigations of inclusion complexes between β-cyclodextrin and alkyl(aqua)cobaloximes (alkyl=butyl, hexyl and cyclohexyl) [J].

Chen, Y ;

Xiang, P ;

Li, G ;

Chen, HL ;

Chinnakali, K ;

Fun, HK .

SUPRAMOLECULAR CHEMISTRY, 2002, 14 (04) :339-346

[7] Molecular recognition in cyclodextrin complexes of amino acid derivatives.: 2.: A new perturbation:: The room-temperature crystallographic structure determination for the N-acetyl-p-methoxy-L-phenylalanine methyl ester/β-cyclodextrin complex [J].

Clark, JL ;

Booth, BR ;

Stezowski, JJ .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2001, 123 (40) :9889-9895

[8] Molecular recognition in cyclodextrin complexes of amino acid derivatives.: 1.: Crystallographic studies of β-cyclodextrin complexes with N-acetyl-L-phenylalanine methyl ester and N-acetyl-L-phenylalanine amide pseudopeptides [J].

Clark, JL ;

Stezowski, JJ .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 2001, 123 (40) :9880-9888

[9] An investigation of the inclusion complex of β-cyclodextrin with 8-nitro-quinoline in the solid state [J].

Fan, Z ;

Diao, CH ;

Yu, M ;

Jing, ZL ;

Chen, X ;

Deng, QL .

SUPRAMOLECULAR CHEMISTRY, 2006, 18 (01) :7-11

[10] CRYSTAL-STRUCTURE OF AN INCLUSION COMPLEX OF BETA-CYCLODEXTRIN WITH RACEMIC FENOPROFEN - DIRECT EVIDENCE FOR CHIRAL RECOGNITION [J].

HAMILTON, JA ;

CHEN, LY .

JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1988, 110 (17) :5833-5841

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