A COMPARATIVE STUDY OF THREE METHODS OF EXTRACTION OF MYCOTOXINS FROM BEER
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作者:
Ionascu, Cosmin
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机构:
West Univ Timisoara, Fac Chem Biol Geog, Dept Biol Chem, Timisoara 300115, RomaniaWest Univ Timisoara, Fac Chem Biol Geog, Dept Biol Chem, Timisoara 300115, Romania
Ionascu, Cosmin
[1
]
Ostafe, Vasile
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机构:
Adv Res Environm Labs, Multidisciplinary Res Platform Nicholas Georgescu, Timisoara 300086, RomaniaWest Univ Timisoara, Fac Chem Biol Geog, Dept Biol Chem, Timisoara 300115, Romania
Ostafe, Vasile
[2
]
机构:
[1] West Univ Timisoara, Fac Chem Biol Geog, Dept Biol Chem, Timisoara 300115, Romania
[2] Adv Res Environm Labs, Multidisciplinary Res Platform Nicholas Georgescu, Timisoara 300086, Romania
来源:
STUDIA UNIVERSITATIS BABES-BOLYAI CHEMIA
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2014年
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59卷
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04期
Three sample preparation methods: solvent extraction, solidphase extraction (SPE) and stir bar sorptive extraction (SBSE) to assess the occurrence of 11 mycotoxins in beer (pale, dark and non-alchoolic) samples were compared. In order to select the best extraction procedure, the sample matrix effects and the effect of the dilution of the sample were investigated by addition of the analytes before and after the extraction procedure was carried out. The study revealed that SPE (with Oasis HLB cartridge) procedure offered the best results compared with the other two extraction methods: relative standard errors under 16% and recovery of the analytes better than 85%. An Ultrahigh Performance Liquid Chromatography coupled with Mass Spectrometry (UPLC-MS/MS) method was used to identify and confirm the mycotoxins.
机构:
College of Life Science & Engineering, Shanxi University of Science & Technology, Xi'an, China
The Research Center of Food Process Engineering Technology in Shaanxi Province, Xi'an, ChinaCollege of Life Science & Engineering, Shanxi University of Science & Technology, Xi'an, China
Zhu, Zhenbao
Liu, Kuang
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College of Life Science & Engineering, Shanxi University of Science & Technology, Xi'an, ChinaCollege of Life Science & Engineering, Shanxi University of Science & Technology, Xi'an, China
Liu, Kuang
Yi, Jianhua
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机构:
College of Life Science & Engineering, Shanxi University of Science & Technology, Xi'an, China
The Research Center of Food Process Engineering Technology in Shaanxi Province, Xi'an, ChinaCollege of Life Science & Engineering, Shanxi University of Science & Technology, Xi'an, China
Yi, Jianhua
Liu, Mengying
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College of Life Science & Engineering, Shanxi University of Science & Technology, Xi'an, ChinaCollege of Life Science & Engineering, Shanxi University of Science & Technology, Xi'an, China
Liu, Mengying
Lu, Yang
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机构:
College of Life Science & Engineering, Shanxi University of Science & Technology, Xi'an, ChinaCollege of Life Science & Engineering, Shanxi University of Science & Technology, Xi'an, China