One-pot solvent-free synthesis of MgFe2O4 nanoparticles from ferrous sulfate waste

被引：14

作者：

Xiang, Hengli ^{[1
,2
]}

Peng, Xu ^{[1
,2
]}

Xu, Dehua ^{[1
,2
]}

Yang, Xiushan ^{[1
,2
]}

Ren, Genkuan ^{[2
,3
]}

Zhang, Zhiye ^{[1
,2
]}

Zhong, Yanjun ^{[1
,2
]}

Wang, Xinlong ^{[1
,2
]}

机构：

[1] Sichuan Univ, Coll Chem Engn, Chengdu 610065, Peoples R China

[2] Minist Educ, Engn Res Ctr Comprehens Utilizat & Clean Proc Pho, Chengdu, Peoples R China

[3] Yibin Univ, Coll Chem & Chem Engn, Yibin, Peoples R China

来源：

MATERIALS AND MANUFACTURING PROCESSES | 2020年 / 35卷 / 05期

关键词：

Magnesium ferrite; nanoparticles; ferrous sulfate waste; solvent-free; MAGNESIUM FERRITE; GREEN SYNTHESIS; XRD; MG;

D O I：

10.1080/10426914.2020.1734617

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

This study proposed a one-pot solvent-free method to synthesize magnesium ferrite nanoparticles using ferrous sulfate waste as raw materials and provided a new idea for high-quality use of ferrous sulfate waste and was promising to be applied in industrialization. Magnesium ferrite nanoparticles (MgFe2O4) were successfully synthesized by a solid-reduction method using ferrous sulfate waste, pyrite and Magnesium carbonate as raw materials. X-ray diffraction (XRD), Fourier transform infrared spectrum (FTIR), scanning electron microscope (SEM), X-ray photoelectron spectroscopy (XPS), Brunauer-Emmett-Teller (BET) method, and superconducting quantum interference device magnetometer were applied to determine the characteristics of obtained samples. The mechanism of synthesizing magnesium ferrite was studied by TGA.

引用

页码：590 / 597

页数：8

共 30 条

[11] Role of Mg in mesoporous MgFe2O4 for efficient catalytic ozonation of Acid Orange II
Lu, Jiang
Wei, Xiaodan
Chang, Yu
Tian, Shuanghong
Xiong, Ya
[J]. JOURNAL OF CHEMICAL TECHNOLOGY AND BIOTECHNOLOGY, 2016, 91 (04) : 985 - 993
[12] Magnesium Ferrite (MgFe2O4) Nanostructures Fabricated by Electrospinning
Maensiri, Santi
Sangmanee, Montana
Wiengmoon, Amporn
[J]. NANOSCALE RESEARCH LETTERS, 2009, 4 (03): : 221 - 228
[13] PREPARATION OF AQUEOUS MAGNETIC LIQUIDS IN ALKALINE AND ACIDIC MEDIA
MASSART, R
[J]. IEEE TRANSACTIONS ON MAGNETICS, 1981, 17 (02) : 1247 - 1248
[14] Synthesis and characterization of manganese ferrite nanoparticles obtained by electrochemical/chemical method
Mazario, E.
Mayoral, A.
Salas, E.
Menendez, N.
Herrasti, P.
Sanchez-Marcos, J.
[J]. MATERIALS & DESIGN, 2016, 111 : 646 - 650
[15] Solid state synthesis of Mg-Ni ferrite and characterization by XRD and XPS
Mittal, VK
Bera, S
Nithya, R
Srinivasan, MP
Velmurugan, S
Narasimhan, SV
[J]. JOURNAL OF NUCLEAR MATERIALS, 2004, 335 (03) : 302 - 310
[16] Solution synthesis and kinetic analyses of the gas sensing characteristics of magnesium ferrite particles
Mukherjee, K.
Bharti, D. C.
Majumder, S. B.
[J]. SENSORS AND ACTUATORS B-CHEMICAL, 2010, 146 (01): : 91 - 97
[17] Effect of Zn-Cr substitution on the structural, magnetic and electrical properties of magnesium ferrite materials
Mulushoa, S. Yonatan
Kumari, Ch Vijaya
Raghavendra, Vemuri
Babu, K. Ephraim
Murthy, B. S. N.
Suribabu, Kundavarapu
Ramakrishna, Y.
Morali, N.
[J]. PHYSICA B-CONDENSED MATTER, 2019, 572 : 139 - 147
[18] Hydrothermal synthesis, structural and impedance studies of nanocrystalline zinc chromite spinel oxide material
Naz, Sumaira
Durrani, Shahid Khan
Mehmood, Mazhar
Nadeem, Muhammad
[J]. JOURNAL OF SAUDI CHEMICAL SOCIETY, 2016, 20 (05) : 585 - 593
[19] A new green synthesis method of magnesium ferrite from ferrous sulfate waste
Peng, Xu
Xu, Dehua
Yang, Xiushan
Zhang, Zhiye
Ren, Genkuan
Yang, Lin
Zhong, Yanjun
Wang, Xinlong
[J]. JOURNAL OF ALLOYS AND COMPOUNDS, 2018, 756 : 117 - 125
[20] Sol-gel route of synthesis of nanoparticles of MgFe2O4 and XRD, FTIR and VSM study
Pradeep, A.
Priyadharsini, P.
Chandrasekaran, G.
[J]. JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2008, 320 (21) : 2774 - 2779

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