One-pot solvent-free synthesis of MgFe2O4 nanoparticles from ferrous sulfate waste

被引：16

作者：

Xiang, Hengli ^{[1
,2
]}

Peng, Xu ^{[1
,2
]}

Xu, Dehua ^{[1
,2
]}

Yang, Xiushan ^{[1
,2
]}

Ren, Genkuan ^{[2
,3
]}

Zhang, Zhiye ^{[1
,2
]}

Zhong, Yanjun ^{[1
,2
]}

Wang, Xinlong ^{[1
,2
]}

机构：

[1] Sichuan Univ, Coll Chem Engn, Chengdu 610065, Peoples R China

[2] Minist Educ, Engn Res Ctr Comprehens Utilizat & Clean Proc Pho, Chengdu, Peoples R China

[3] Yibin Univ, Coll Chem & Chem Engn, Yibin, Peoples R China

来源：

MATERIALS AND MANUFACTURING PROCESSES | 2020年 / 35卷 / 05期

关键词：

Magnesium ferrite; nanoparticles; ferrous sulfate waste; solvent-free; MAGNESIUM FERRITE; GREEN SYNTHESIS; XRD; MG;

D O I：

10.1080/10426914.2020.1734617

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

This study proposed a one-pot solvent-free method to synthesize magnesium ferrite nanoparticles using ferrous sulfate waste as raw materials and provided a new idea for high-quality use of ferrous sulfate waste and was promising to be applied in industrialization. Magnesium ferrite nanoparticles (MgFe2O4) were successfully synthesized by a solid-reduction method using ferrous sulfate waste, pyrite and Magnesium carbonate as raw materials. X-ray diffraction (XRD), Fourier transform infrared spectrum (FTIR), scanning electron microscope (SEM), X-ray photoelectron spectroscopy (XPS), Brunauer-Emmett-Teller (BET) method, and superconducting quantum interference device magnetometer were applied to determine the characteristics of obtained samples. The mechanism of synthesizing magnesium ferrite was studied by TGA.

引用

页码：590 / 597

页数：8

共 30 条

[11] Role of Mg in mesoporous MgFe2O4 for efficient catalytic ozonation of Acid Orange II [J].

Lu, Jiang ;

Wei, Xiaodan ;

Chang, Yu ;

Tian, Shuanghong ;

Xiong, Ya .

JOURNAL OF CHEMICAL TECHNOLOGY AND BIOTECHNOLOGY, 2016, 91 (04) :985-993

[12] Magnesium Ferrite (MgFe2O4) Nanostructures Fabricated by Electrospinning [J].

Maensiri, Santi ;

Sangmanee, Montana ;

Wiengmoon, Amporn .

NANOSCALE RESEARCH LETTERS, 2009, 4 (03) :221-228

[13] PREPARATION OF AQUEOUS MAGNETIC LIQUIDS IN ALKALINE AND ACIDIC MEDIA [J].

MASSART, R .

IEEE TRANSACTIONS ON MAGNETICS, 1981, 17 (02) :1247-1248

[14] Synthesis and characterization of manganese ferrite nanoparticles obtained by electrochemical/chemical method [J].

Mazario, E. ;

Mayoral, A. ;

Salas, E. ;

Menendez, N. ;

Herrasti, P. ;

Sanchez-Marcos, J. .

MATERIALS & DESIGN, 2016, 111 :646-650

[15] Solid state synthesis of Mg-Ni ferrite and characterization by XRD and XPS [J].

Mittal, VK ;

Bera, S ;

Nithya, R ;

Srinivasan, MP ;

Velmurugan, S ;

Narasimhan, SV .

JOURNAL OF NUCLEAR MATERIALS, 2004, 335 (03) :302-310

[16] Solution synthesis and kinetic analyses of the gas sensing characteristics of magnesium ferrite particles [J].

Mukherjee, K. ;

Bharti, D. C. ;

Majumder, S. B. .

SENSORS AND ACTUATORS B-CHEMICAL, 2010, 146 (01) :91-97

[17] Effect of Zn-Cr substitution on the structural, magnetic and electrical properties of magnesium ferrite materials [J].

Mulushoa, S. Yonatan ;

Kumari, Ch Vijaya ;

Raghavendra, Vemuri ;

Babu, K. Ephraim ;

Murthy, B. S. N. ;

Suribabu, Kundavarapu ;

Ramakrishna, Y. ;

Morali, N. .

PHYSICA B-CONDENSED MATTER, 2019, 572 :139-147

[18] Hydrothermal synthesis, structural and impedance studies of nanocrystalline zinc chromite spinel oxide material [J].

Naz, Sumaira ;

Durrani, Shahid Khan ;

Mehmood, Mazhar ;

Nadeem, Muhammad .

JOURNAL OF SAUDI CHEMICAL SOCIETY, 2016, 20 (05) :585-593

[19] A new green synthesis method of magnesium ferrite from ferrous sulfate waste [J].

Peng, Xu ;

Xu, Dehua ;

Yang, Xiushan ;

Zhang, Zhiye ;

Ren, Genkuan ;

Yang, Lin ;

Zhong, Yanjun ;

Wang, Xinlong .

JOURNAL OF ALLOYS AND COMPOUNDS, 2018, 756 :117-125

[20] Sol-gel route of synthesis of nanoparticles of MgFe2O4 and XRD, FTIR and VSM study [J].

Pradeep, A. ;

Priyadharsini, P. ;

Chandrasekaran, G. .

JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, 2008, 320 (21) :2774-2779

← 1 2 3 →