Synthesis and Crystal Structure of N-Cyclohexyl-2-Nitrobenzamide

被引：0

作者：

Saeed, Aamer ^{[1
]}

Hussain, Shahid ^{[1
]}

Bolte, Michael ^{[2
]}

机构：

[1] Quaid I Azam Univ, Dept Chem, Islamabad 45320, Pakistan

[2] Goethe Univ Frankfurt, Inst Anorgan Chem, D-60438 Frankfurt, Germany

来源：

JOURNAL OF CHEMICAL CRYSTALLOGRAPHY | 2010年 / 40卷 / 11期

关键词：

X-ray structure; N-Cyclohexyl-2-nitrobenzamide; Synthesis;

D O I：

10.1007/s10870-010-9764-0

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

N-Cyclohexyl-2-nitrobenzamide was synthesized and characterized by spectroscopic data and X-ray diffraction analysis It crystallizes at room temperature in the monoclinic space group P21/n with cell parameters a = 13 9913(10), b = 8 8475(4), c = 20 5627(15) angstrom, beta = 93 278(6)degrees, V 2541 3(3) A(3) and Z = 8 The structure was refined to final R1 = 0 0626 using all 4950 reflections The crystal packing is stabilized by N-H O hydrogen bonds

引用

页码：924 / 926

页数：3

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