Preparation of nanosized anatase TiO2 powder with high thermal stability

被引:0
作者
Zhao, WK [1 ]
Fang, YL
Zhang, KC
Wang, YZ
机构
[1] Wuhan Univ, Dept Chem, Wuhan 430072, Peoples R China
[2] Wuhan Food Ind Coll, Wuhan 430022, Peoples R China
[3] Chinese Acad Sci, Ecoenvironm Sci Res Ctr, State Key Lab Environm Aquat Chem, Beijing 100085, Peoples R China
关键词
titanium dioxide; nanosized powder; organic media; preparation and characterization;
D O I
暂无
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Nanosized anatase TiO2 powder was prepared by the high-temperature hydrolysis of titanium tetrabutoxide and crystallization in the organic media. The nanosized powder was characterization by XRD, BET, TEM, TG and DTA methods. The powder remains anatase crystallites in a wide temperature range (200 similar to 700 degrees C). The average diameter of the nanosized TiO2 powder after calcination at 550 degrees C is 14nm and the specific surface is >100m(2)/g.
引用
收藏
页码:608 / 612
页数:5
相关论文
共 6 条
[1]  
DOUGLAS C, 1994, J AM CERAM SOC, V77, P1957
[2]  
KEIICHI T, 1991, CHEM PHYS LETT, V187, P73
[3]  
Klug H.P., 1974, XRAY DIFFRACTION PRO, VSecond, P618
[4]   PREPARATION AND CHARACTERIZATION OF TITANIUM(IV) OXIDE PHOTOCATALYSTS [J].
LEE, W ;
GAO, YM ;
DWIGHT, K ;
WOLD, A .
MATERIALS RESEARCH BULLETIN, 1992, 27 (06) :685-692
[5]  
Poniatowski E.H., 1994, J MATER RES, V9, P2102
[6]  
Robert A.S., 1957, ANAL CHEM, V29, P760