Evaluation of different rectangular scan strategies for STEM imaging

被引:16
|
作者
Velazco, A. [1 ,2 ]
Nord, M. [1 ,2 ]
Beche, A. [1 ,2 ]
Verbeeck, J. [1 ,2 ]
机构
[1] Univ Antwerp, EMAT, Groenenborgerlaan 171, B-2020 Antwerp, Belgium
[2] Univ Antwerp, NANOlab Ctr Excellence, Antwerp, Belgium
关键词
Aberration corrected STEM; Scanning distortions; Drift; Precision; Hilbert scan pattern; DISTORTION CORRECTION; ELECTRON;
D O I
10.1016/j.ultramic.2020.113021
中图分类号
TH742 [显微镜];
学科分类号
摘要
STEM imaging is typically performed by raster scanning a focused electron probe over a sample. Here we in- vestigate and compare three different scan patterns, making use of a programmable scan engine that allows to arbitrarily set the sequence of probe positions that are consecutively visited on the sample. We compare the typical raster scan with a so-called ?snake ? pattern where the scan direction is reversed after each row and a novel Hilbert scan pattern that changes scan direction rapidly and provides an homogeneous treatment of both scan directions. We experimentally evaluate the imaging performance on a single crystal test sample by varying dwell time and evaluating behaviour with respect to sample drift. We demonstrate the ability of the Hilbert scan pattern to more faithfully represent the high frequency content of the image in the presence of sample drift. It is also shown that Hilbert scanning provides reduced bias when measuring lattice parameters from the obtained scanned images while maintaining similar precision in both scan directions which is especially important when e.g. performing strain analysis. Compared to raster scanning with flyback correction, both snake and Hilbert scanning benefit from dose reduction as only small probe movement steps occur.
引用
收藏
页数:10
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