Ultrasound-promoted an efficient method for the one-pot synthesis of indeno fused pyrido[2,3-d] pyrimidines catalyzed by H3PW12O40 functionalized chitosan@Co3O4 as a novel and green catalyst

被引：18
|
作者：
Safari, Javad [1 ]
Tavakoli, Mona [1 ]
Ghasemzadeh, Mohammad Ali [2 ]
机构：
[1] Univ Kashan, Dept Organ Chem, Fac Chem, Kashan 87317, Iran
[2] Islamic Azad Univ, Qom Branch, Dept Chem, Qom, Iran
来源：
JOURNAL OF ORGANOMETALLIC CHEMISTRY | 2019年 / 880卷
关键词：
Heterogeneous catalyst; Co3O4/CS/PWA; Three-component reaction; Ultrasound irradiation; Indeno[2 '; 1; :5,6] pyrido[ 2,3-d] pyrimidine; ENCAPSULATED-SILICA PARTICLES; SULFONIC-ACID; NANOPARTICLES; ANTIBACTERIAL; NANOCATALYST; WATER; HETEROPOLYACIDS; REDUCTION; ALDEHYDES;
D O I：
10.1016/j.jorganchem.2018.10.028
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A novel magnetically recoverable nanocomposite including Co3O4/chitosan/H3PW12O40 (Co3O4/CS/PWA) as a heterogeneous catalyst was prepared using a facile synthetic method and characterized by FT-IR, XRD, SEM, VSM and EDX. A simple, efficient and rapid synthesis of indeno[2',1':5,6] pyrido[2,3-d] pyrimidines was accomplished in excellent yields via one-pot three-component reaction of 1,3-dimethyl-6-aminouracil, aryl aldehydes and 1,3-indandione in the presence of amount of Co3O4/CS/PWA catalyst under ultrasound irradiation. Then, the catalyst was recovered with an external magnet and reused several times without significant loss of reactivity. (C) 2018 Published by Elsevier B.V.
引用
收藏
页码：75 / 82
页数：8
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