Continuous Synthesis of Hydrogenated Graphene in Thermal Plasma

被引:2
作者
Shavelkina, M. B. [1 ]
Amirov, R. Kh. [1 ]
Alikhanov, N. R. [2 ]
Vakhitov, I. R. [3 ]
Shatalova, T. B. [4 ]
机构
[1] Russian Acad Sci, Joint Inst High Temp, Moscow, Russia
[2] Dagestan State Univ, Makhachkala, Russia
[3] Kazan Fed Univ, Inst Phys, Kazan, Russia
[4] Lomonosov Moscow State Univ, Moscow, Russia
关键词
plasma torch; plasma jet; plasma chemistry; conversion; methane; synthesis; graphene; hydrogenated graphene; helium; CHEMICAL-VAPOR-DEPOSITION; ARC-DISCHARGE; GRAPHITE; CARBON; FILMS;
D O I
10.1134/S0022476618040042
中图分类号
O61 [无机化学];
学科分类号
070301 ; 081704 ;
摘要
A single-stage catalyst free synthesis of hydrogenated graphene was studied in the process of methane conversion in a helium plasma jet created by a plasma torch at the power up to 45 kW and the pressure of 710 Torr. The synthesis products were studied by the methods of scanning and transmission electron microscopy, thermal analysis, Raman spectroscopy, X-ray photoelectron spectroscopy, and X-ray diffraction analysis.
引用
收藏
页码:773 / 779
页数:7
相关论文
共 30 条
  • [1] Synthesis of high-purity multilayer graphene using plasma jet
    Amirov, R. H.
    Iskhakov, M. E.
    Shavelkina, M. B.
    [J]. NANOSYSTEMS-PHYSICS CHEMISTRY MATHEMATICS, 2016, 7 (01): : 60 - 64
  • [2] Advanced anticorrosive coatings prepared from electroactive polyimide/graphene nanocomposites with synergistic effects of redox catalytic capability and gas barrier properties
    Chang, K. C.
    Hsu, C. H.
    Lu, H. I.
    Ji, W. F.
    Chang, C. H.
    Li, W. Y.
    Chuang, T. L.
    Yeh, J. M.
    Liu, W. R.
    Tsai, M. H.
    [J]. EXPRESS POLYMER LETTERS, 2014, 8 (04): : 243 - 255
  • [3] Interaction of graphite with atomic hydrogen
    Denisov, EA
    Kompaniets, TN
    [J]. TECHNICAL PHYSICS, 2001, 46 (02) : 240 - 244
  • [4] Raman spectrum of graphene and graphene layers
    Ferrari, A. C.
    Meyer, J. C.
    Scardaci, V.
    Casiraghi, C.
    Lazzeri, M.
    Mauri, F.
    Piscanec, S.
    Jiang, D.
    Novoselov, K. S.
    Roth, S.
    Geim, A. K.
    [J]. PHYSICAL REVIEW LETTERS, 2006, 97 (18)
  • [5] Raman spectroscopy of graphene and graphite: Disorder, electron-phonon coupling, doping and nonadiabatic effects
    Ferrari, Andrea C.
    [J]. SOLID STATE COMMUNICATIONS, 2007, 143 (1-2) : 47 - 57
  • [6] Plasma pyrolysis of methane to hydrogen and carbon black
    Fincke, JR
    Anderson, RP
    Hyde, TA
    Detering, BA
    [J]. INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH, 2002, 41 (06) : 1425 - 1435
  • [7] Dynamic mechanical behavior of multilayer graphene via supersonic projectile penetration
    Lee, Jae-Hwang
    Loya, Phillip E.
    Lou, Jun
    Thomas, Edwin L.
    [J]. SCIENCE, 2014, 346 (6213) : 1092 - 1096
  • [8] The large-scale production of graphene flakes using magnetically-enhanced arc discharge between carbon electrodes
    Levchenko, I.
    Volotskova, O.
    Shashurin, A.
    Raitses, Y.
    Ostrikov, K.
    Keidar, M.
    [J]. CARBON, 2010, 48 (15) : 4570 - 4574
  • [9] Li J., 2012, Graphene, V1, P1, DOI [DOI 10.4236/GRAPHENE.2012.11001, 10.4236/graphene.2012.11001]
  • [10] Li J., 2012, J VIS EXP, V60, P3455