Annealing protocols for pyrrolidinium bis(trifluoromethylsulfonyl)imide type ionic liquids

被引：22

作者：

Furlani, M. ^{[1
]}

Albinsson, I. ^{[2
]}

Mellander, B. -E. ^{[1
]}

Appetecchi, G. B. ^{[3
]}

Passerini, S. ^{[3
,4
]}

机构：

[1] Chalmers Univ Technol, Dept Appl Phys, S-41296 Gothenburg, Sweden

[2] Univ Gothenburg, Dept Phys, S-41296 Gothenburg, Sweden

[3] UTRINN IFC, Italian Natl Agcy New Technol Energy & Sustainabl, ENEA, I-00123 Rome, Italy

[4] Univ Munster, Inst Phys Chem, D-48149 Munster, Germany

来源：

ELECTROCHIMICA ACTA | 2011年 / 57卷

关键词：

Ionic liquids; DSC; Annealing; PHASE-BEHAVIOR;

D O I：

10.1016/j.electacta.2011.08.056

中图分类号：

O646 [电化学、电解、磁化学];

学科分类号：

081704 ;

摘要：

The phase transitions in ionic liquids (ILs) of the N-alkyl-N-methylpyrrolidinium bis(trifluoromethanesulfonyl)imide (PYR1ATFSI) family show a common pattern, which implies a typical and characteristic crystal packing. Many of these features are also observed for the N-alkyl-N-methylpiperidinium bis(trifluoromethanesulfonyl)imide (PIP1ATFSI) family. Here we report the thermal behavior of some ILs of the PYR1ATFSI and PIP1ATFSI families and a few others having different anions. The thermal history was found to decide which phases will appear and, therefore, specific protocols were defined to obtain the desired phases in a reasonable amount of time. (C) 2011 Elsevier Ltd. All rights reserved.

引用

页码：220 / 227

页数：8

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