Synthesis and characterization of poly thiophene-2-carbaldehyde by hydrochloric acid as catalyst

被引：2

作者：

Al-Hamdan, Ahmad ^{[1
]}

Al-Falah, Ahmad ^{[1
,2
]}

Al-Deri, Fawaz ^{[1
]}

机构：

[1] Damascus Univ, Dept Chem, Damascus, Syria

[2] Fac Pharm Arab Int, Damascus, Syria

来源：

KUWAIT JOURNAL OF SCIENCE | 2021年 / 48卷 / 03期

关键词：

EDX; polymers characterization; thiophene; thiophene-2-carbaldehyde; XPS;

D O I：

10.48129/kjs.v48i3.9624

中图分类号：

O [数理科学和化学]; P [天文学、地球科学]; Q [生物科学]; N [自然科学总论];

学科分类号：

07 ; 0710 ; 09 ;

摘要：

Poly thiophene and its derivatives are important conductive polymers because of their wide applications. They were polymerized by chemical and electrochemical methods. In this paper, thiophene-2-carbaldehyde was polymerized by hydrochloric acid as a catalyst in alcohol as a solvent. The resulting polymer was characterized by (FT/IR, H-1-NMR, EDX, and XPS) to determine the polymer structure. The resulting polymer was scanned by scanning electron microscope (SEM) for its morphological properties. We found the polymer consisting of spherical particles with a rough surface (average diameters of 127 nanometers) that clump together and form clusters

引用

页数：6

共 50 条

[31] Preparation of octahydro-2H-chromen-4-ol with analgesic activity from isopulegol and thiophene-2-carbaldehyde in the presence of acid-modified clays
Sidorenko, A. Yu.
Kravtsova, A. V.
Warna, J.
Aho, A.
Heinmaa, I.
Il'ina, I. V.
Ardashov, O. V.
Volcho, K. P.
Salakhutdinov, N. F.
Murzin, D. Yu.
Agabekov, V. E.
MOLECULAR CATALYSIS, 2018, 453 : 139 - 148
[32] Synthesis, spectroscopy and structures of halogen and sulfur-bridged dinuclear silver(I) complexes with N1-substituted thiophene-2-carbaldehyde thiosemicarbazone
Lobana, Tarlok S.
Sharma, Rekha
Butcher, Ray J.
POLYHEDRON, 2009, 28 (06) : 1103 - 1110
[33] Reactions of 2,2,6-Trimethyl-1,3-dioxin-4-one with the Aryl Aldimines Prepared from Thiophene-2-carbaldehyde
Koser, Ilayda
Ocal, Nuket
Erden, Ihsan
JOURNAL OF HETEROCYCLIC CHEMISTRY, 2017, 54 (03) : 1828 - 1832
[34] Design, Synthesis, Biocompatibility, molecular docking and molecular dynamics studies of novel Benzo[b]thiophene-2-carbaldehyde derivatives targeting human IgM Fc Domains
Rajimon, K. J.
Alzahrani, Abdullah Yahya Abdullah
Thangaiyan, Pooventhiran
Thomas, Renjith
BIOORGANIC CHEMISTRY, 2025, 156
[35] 5-(N-Ethylcarbazol-3-yl)thiophene-2-carbaldehyde (ECTC): a novel fluorescent sensor for ferric ion
Zhang, Qiang
Wei, Huaixin
Zhai, Rongjia
Ji, Zhongling
Qi, Yu
Zhao, Xin
HETEROCYCLIC COMMUNICATIONS, 2016, 22 (05) : 287 - 290
[36] Synthesis and characterization of high performance poly(thiophene).
Graham, J
Jin, S
Harris, FW
Cheng, SZD
Bunning, TJ
ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2004, 228 : U338 - U338
[37] CALORIMETRIC DETERMINATION OF ENTHALPY OF O-]N-ACYL REARRANGEMENT IN IMINES OF 3-ACETOXYBENZO[B]THIOPHENE-2-CARBALDEHYDE
POPOVA, LL
PALUI, GD
SUSLOV, AN
BREN, VA
MINKIN, VI
ZHURNAL FIZICHESKOI KHIMII, 1989, 63 (03): : 587 - 590
[38] Synthesis and characterization of poly(3-thiophene acetic acid) upon binding by cationic groups
Nguyen Ngoc Linh
Tran Minh Thi
Duong Khanh Linh
Vu Thi Huong
Ha Manh Hung
Doan Thi Yen Oanh
Vu Quoc Trung
VIETNAM JOURNAL OF CHEMISTRY, 2021, 59 (06) : 902 - 909
[39] Synthesis and structures of monomeric [chloro(isatin-3-thiosemicarbazone)bis(triphenylphosphine)]copper(I) and dimeric [dichlorobis(thiophene-2-carbaldehyde thiosemicarbazone)bis(triphenylphosphine)]dicopper(I)] complexes
Lobana, Tarlok S.
Rekha
Pannu, A. P. S.
Hundal, Geeta
Butcher, Ray J.
Castineiras, A.
POLYHEDRON, 2007, 26 (12) : 2621 - 2628
[40] Microwave-assisted synthesis of malic acid involving hydrochloric acid as catalyst
Pacheco Ortiz, Ronald Wbeimar
de Jesus, Brendha Goncalves
Franceschi, Elton
Dariva, Claudio
Cardozo-Filho, Lucio
Zanoelo, Everton Fernando
REACTION KINETICS MECHANISMS AND CATALYSIS, 2017, 122 (02) : 793 - 802

← 1 2 3 4 5 →