GC/MS identification of some dibutyl phthalates hydrogenation products

被引：0

作者：

Dziwinski, Euzebiusz J. ^{[1
]}

Tasarska, Aleksandra

Lach, Jozef ^{[1
]}

机构：

[1] Inst Ciezkiej Syntezy Organicznej Blachownia, PL-47225 Kedzierzyn Kozle, Poland

来源：

PRZEMYSL CHEMICZNY | 2010年 / 89卷 / 10期

关键词：

D O I：

暂无

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Bu(2) and iso-Bu(2) phthalates were hydrogenated on Ni catalyst to resp. cyclohexane-1,2-dicarboxylates. The reaction product was analyzed by gas chromatography coupled with mass spectrometry. Beside of cis and trans isomers of the main product, the presence of small amts. (below 0.1% by mass) of BuOH, i-BuOH, Bu benzoates, cyclohexanecarboxylates and 2-methylbenzoates as well as phthalide of cyclohexane-1,2-dicarboxylic acid was evidenced.

引用

页码：1305 / 1308

页数：4

共 50 条

[21] An optimized method for the identification of pesticides in cannabis products using GC/MS with AMDIS [J].

Cochran, Katie ;

Harris, Heather .

ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2018, 255

[22] Diazinon decomposition by soil bacteria and identification of degradation products by GC-MS [J].

Thabit, Tamer Mohamed Ahmed Mohamed ;

El-Naggar, Medhat Ahmed Hassan .

SOIL & ENVIRONMENT, 2013, 32 (02) :96-102

[23] Human risk assessment and GC/MS analysis of phthalates in excipients for pharmaceuticals [J].

Kim, Hyung-Sik ;

Hyeon, Ji-Hyeon ;

Shin, Min-Kyung ;

Park, Hyun-Jong ;

Lee, Jung-Dae ;

Kim, Ji-Yun ;

Gwak, Hyo-Min ;

Um, Yoon-Mi ;

Son, Ji-Yeon ;

Kim, Kyeong-Seok ;

Sachan, Richa ;

De, Umasankar ;

Kang, Yoon-Jong ;

Lee, Byung-Mu .

TOXICOLOGY LETTERS, 2014, 229 :S104-S104

[24] MORE ON GC MS IDENTIFICATION [J].

STEVENS, AA .

ENVIRONMENTAL SCIENCE & TECHNOLOGY, 1982, 16 (11) :A595-A596

[25] GUIDELINES FOR GC MS IDENTIFICATION [J].

CHRISTMAN, RF .

ENVIRONMENTAL SCIENCE & TECHNOLOGY, 1982, 16 (03) :A143-A143

[26] Identification of arsenolipids with GC/MS [J].

Raber, Georg ;

Khoomrung, Sakda ;

Taleshi, Mojtaba S. ;

Edmonds, John S. ;

Francesconi, Kevin A. .

TALANTA, 2009, 78 (03) :1215-1218

[27] THE IDENTIFICATION OF COCAINE IN HAIR BY GC/MS AND MS/MS [J].

MARTZ, RM .

CRIME LABORATORY DIGEST, 1988, 15 (03) :67-73

[28] IDENTIFICATION OF MICROORGANISMS BY GC/MS [J].

WARNER, MD .

ANALYTICAL CHEMISTRY, 1986, 58 (13) :1310-&

[29] Identification of Diesel Residues by GC/MS/MS [J].

Liu, Shujun ;

Wang, Bai ;

Wang, Ying .

2ND INTERNATIONAL CONFERENCE ON NEW ENERGY AND RENEWABLE RESOURCES (ICNERR 2017), 2017, :341-345

[30] IDENTIFICATION AND DETERMINATION OF SOME DEGRADATION PRODUCTS OF MANCOZEB BY HPLC AND MS [J].

LEHOTAY, J ;

HOLOTIK, S ;

BRANDSTETEROVA, E .

JOURNAL OF LIQUID CHROMATOGRAPHY, 1992, 15 (13) :2397-2405

← 1 2 3 4 5 →