ECO-FRIENDLY ONE-POT SYNTHESIS OF 2,4-DISUBSTITUTED THIAZOLES BY GRINDING UNDER CATALYST-AND SOLVENT-FREE CONDITIONS

被引：15
|
作者：
Ding, Quansehng [1 ]
Zhu, Dongjian [1 ]
Jin, Huile [1 ]
Chen, Jiuxi [1 ]
Ding, Jinchang [1 ]
Wu, Huayue [1 ]
机构：
[1] Wenzhou Univ, Coll Chem & Mat Engn, Wenzhou 325027, Peoples R China
来源：
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2011年 / 186卷 / 02期
关键词：
Catalyst-free; grinding; one-pot; solvent-free; thiazoles; EFFICIENT SYNTHESIS; 2-AMINOTHIAZOLES; AMINOTHIAZOLES; DERIVATIVES; DISULFIDES; CHLORIDE;
D O I：
10.1080/10426507.2010.492366
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
An efficient and facile synthesis of 2,4-disubstituted thiazoles is achieved by a one-pot reaction of aldehydes and alpha-bromoketones with thiosemicarbazide by grinding under catalyst-and solvent-free conditions. This method has notable advantages in terms of simple workup, neat conditions, high yield, reasonably rapid reaction rate, and environmental friendliness.
引用
收藏
页码：220 / 224
页数：5
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