Hydroxyapatite coatings containing Zn and Si on Ti-6Al-4Valloy by plasma electrolytic oxidation

被引:32
作者
Hwang, In-Jo
Choe, Han-Cheol [1 ,2 ]
机构
[1] Chosun Univ, Dept Dent Mat, Coll Dent, Gwangju, South Korea
[2] Chosun Univ, Res Ctr Nanointerface Activat Biomat, Coll Dent, Gwangju, South Korea
关键词
Hydroxyapatite; Zinc (Zn); Silicon (Si); Plasma electrolytic oxidation (PEO); Electrolyte; SURFACE TREATMENTS; CALCIUM-PHOSPHATE; ALLOYS; TITANIUM; DEPOSITION; FILMS; ZINC;
D O I
10.1016/j.apsusc.2017.01.313
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
In this study, hydroxyapatite coatings containing Zn and Si on Ti-6Al-4Valloy by plasma electrolytic oxidation were researched using various experimental instruments. The pore size is depended on the electrolyte concentration and the particle size and number of pore increase on surface part and pore part. In the case of Zn/Si sample, pore size was larger than that of Zn samples. The maximum size of pores decreased and minimum size of pores increased up to 10Zn/Si and Zn and Si affect the formation of pore shapes. As Zn ion concentration increases, the size of the particle tends to increase, the number of particles on the surface part is reduced, whereas the size of the particles and the number of particles on pore part increased. Zn is mainly detected at pore part, and Si is mainly detected at surface part. The crystallite size of anatase increased as the Zn ion concentration, whereas, in the case of Si ion added, crystallite size of anatase decreased. (C) 2017 Elsevier B.V. All rights reserved.
引用
收藏
页码:337 / 346
页数:10
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