Single-Laboratory Validation Study of Simple and Simultaneous Determination Method for Pesticide Residues in Meat by LC-MS/MS

被引：2

作者：

Sasamoto, Takeo ^{[1
]}

Kobayashi, Maki ^{[1
]}

Sakai, Naoko ^{[1
]}

Kamijo, Kyoko ^{[1
]}

Ootani, Harunori ^{[1
]}

Hayashi, Masaki ^{[1
]}

Baba, Itoko ^{[1
]}

Hanashiro, Chikako ^{[1
]}

Takano, Ichiro ^{[1
]}

机构：

[1] Tokyo Metropolitan Inst Publ Hlth, Shinjuku Ku, Tokyo 1690073, Japan

来源：

FOOD HYGIENE AND SAFETY SCIENCE | 2015年 / 56卷 / 01期

关键词：

pesticide residue; simultaneous determination method; simple determination method; single-laboratory validation study; LC-MS/MS; MULTICLASS VETERINARY DRUGS; RAPID ANALYSIS METHOD; PRODUCTS; CHROMATOGRAPHY; EXTRACTION; CLEANUP;

D O I：

10.3358/shokueishi.56.19

中图分类号：

TS2 [食品工业];

学科分类号：

0832 ;

摘要：

We performed a single-laboratory validation study of a simple and simultaneous determination method for pesticide residues in meat using LC-MS/MS. Water was added to the sample and the mixture was homogenized. Next, pesticides were extracted with acetonitrile containing 1 vol% formic acid using a homogenizer, and salted out with magnesium sulfate, trisodium citrate and sodium chloride. After centrifugation, the acetonitrile layer was made up to standard volume and analyzed by LC-MS/MS. This method was assessed by performing recovery tests in retail bovine, swine and chicken muscle samples spiked with the 132 pesticides at the levels of 0.01 and 0.04 mu g/g. Among them, 125 pesticides satisfied the Japanese method validation guideline criteria in bovine, 120 in swine and 127 in chicken.

引用

页码：19 / 30

页数：12

共 14 条

[1]

Anastassiades M, 2003, J AOAC INT, V86, P412

[2] Study of Multi-residue Method for Determining Pesticide Residues in Processed Foods Manufactured from Agricultural Products by LC-MS/MS [J].

Fukui, Naoki ;

Takatori, Satoshi ;

Kitagawa, Yoko ;

Okihashi, Masahiro ;

Kajimura, Keiji ;

Obana, Hirotaka .

FOOD HYGIENE AND SAFETY SCIENCE, 2013, 54 (06) :426-433

[3]

Hashimoto T., 2003, ANN REPORT TOKYO MET, V54, P171

[4]

Hashimoto T., 2005, ANN REPORT TOKYO MET, V56, P211

[5]

Hashimoto T., 2004, ANN REPORT TOKYO MET, V55, P221

[6] New Clean-up Method with Dispersive Solid-Phase Extraction for Simultaneous Determination of Pesticide Residues in Livestock Products by GC-MS/MS [J].

Kondo, Takahide ;

Kaburagi, Yasuo ;

Shibata, Masahisa ;

Kurokawa, Chieko ;

Inoue, Yutaka ;

Yamamoto, Yoshihiko ;

Miyazaki, Motonobu .

FOOD HYGIENE AND SAFETY SCIENCE, 2012, 53 (02) :75-84

[7] Screening Method of Pesticides in Meat using Cleanup with GPC and Mini-column [J].

Matsuoka, Tomofumi ;

Akiyama, Yumi ;

Mitsuhashi, Takao .

JOURNAL OF THE FOOD HYGIENIC SOCIETY OF JAPAN, 2009, 50 (02) :97-107

[8]

NAGAYAMA T, 1994, J FOOD HYG SOC JPN, V35, P470, DOI 10.3358/shokueishi.35.470

[9]

Nakajima T, 2013, FOOD HYG SAFE SCI, V54, P335, DOI 10.3358/shokueishi.54.335

[10] Development and Validation of Rapid Analysis Method for Multi-Class Veterinary Drugs in Livestock Products by LC-MS/MS [J].

Nakajima, Takayuki ;

Nagano, Chieko ;

Sasamoto, Takeo ;

Hayashi, Hiroshi ;

Kanda, Maki ;

Kanai, Setsuko ;

Takeba, Kazue ;

Matsushima, Yoko ;

Takano, Ichiro .

FOOD HYGIENE AND SAFETY SCIENCE, 2012, 53 (05) :243-253

← 1 2 →