X-ray powder diffraction data and structural refinement of Er3Co6Sn5

被引:0
作者
He, W
Zeng, LM
Qin, W
Yan, JL
Hao, JM
机构
[1] Univ Sci & Technol China, Ctr Fundamental Phys, Hefei 230026, Peoples R China
[2] Guangxi Univ, Inst Mat Sci, Nanning 530004, Peoples R China
[3] Tianjin Elect Mat Res Inst, Tianjin 300192, Peoples R China
关键词
Er2Co6Sn5; X-ray powder diffraction; Rietveld structural refinement;
D O I
暂无
中图分类号
TF [冶金工业];
学科分类号
0806 ;
摘要
The compound Er3Co6Sn5 has been studied by means of X-ray powder diffraction technique and refined by Rietveld method. The compound Er3Co6Sn5 has an orthorhombic Dy3Co6Sn5-type structure, space group Immm (No. 71), Z = 2 and D-x = 9.465 g/cm(3). At room temperature, the lattice constants are a = 4.296 6(4) Angstrom, b = 12. 289 7(9) Angstrom, c = 9.627 1(6)Angstrom. The Rietveld structural refinement was performed and led to R-wp = 0. 196 and R-p = 0.153. The figure of merit F-N for the X-ray powder diffraction data is F-30 = 34.7 (0.009 0, 96). The present structural refinement supports that Er(1), Er(2), Co(1), Co(2), Sn (i) and Sn(2) atoms occupy the 2 a, 4 g, 4 j, 8 l, 2 c and 8 l positions, respectively.
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页码:86 / 88
页数:3
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