[PPh4]2[Pd{Se2C2(COOCH3)2}2]

被引：2

作者：

McLauchlan, CC ^{[1
]}

Ibers, JA ^{[1
]}

机构：

[1] Northwestern Univ, Dept Chem, Evanston, IL 60208 USA

来源：

ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1999年 / 55卷

关键词：

D O I：

10.1107/S0108270198010543

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The title compound, bis(tetraphenylphosphonium) bis(cis-1,2- dicarbomethoxyethylene-1,2-diseleno) palladate(II) {alternative name: bis(tetraphenylphosphonium) bis[dimethyl 2,3-bis(selenido)but-2-ene-1 4-dioato-Se,Se']-palladate(II)}, (C24H20P)(2)[Pd(C6H6O4Se2)(2)], shows a similar structure to the telluro, seleno, and sulfide analogues with other transition metals.

引用

页码：30 / 32

页数：3

共 9 条

[1] REACTION OF DIMETHYL ACETYLENEDICARBOXYLATE WITH WSE92- AND W2SE102- - SYNTHESIS AND CHARACTERIZATION OF THE [W(SE2C2(COOCH3)2)3]2- AND [W2SE2(SE2C2(COOCH3)2)4]2- [J].

ANSARI, MA ;

MAHLER, CH ;

IBERS, JA .

INORGANIC CHEMISTRY, 1989, 28 (13) :2669-2674

[2] SYNTHESIS, STRUCTURE, SPECTROSCOPY, AND REACTIVITY OF NI(SE4)22-, PD(SE4)22-, ZN(SE4)22-, CD(SE4)22-, HG(SE4)22-, AND MN(SE4)22- ANIONS [J].

ANSARI, MA ;

MAHLER, CH ;

CHORGHADE, GS ;

LU, YJ ;

IBERS, JA .

INORGANIC CHEMISTRY, 1990, 29 (19) :3832-3839

[3] TEMPLATE SYNTHESES OF 1,2-ALKENE DICHALCOGENIDE CHELATES VIA THE ADDITION OF ACTIVATED ACETYLENES TO DICYCLOPENTADIENYLTITANIUM PENTACHALCOGENIDES [J].

BOLINGER, CM ;

RAUCHFUSS, TB .

INORGANIC CHEMISTRY, 1982, 21 (11) :3947-3954

[4] ABSORPTION CORRECTION IN CRYSTAL STRUCTURE ANALYSIS [J].

DEMEULENAER, J ;

TOMPA, H .

ACTA CRYSTALLOGRAPHICA, 1965, 19 :1014-+

[5] CHEMISTRY OF HIGH-VALENT TRANSITION-METAL POLYTELLURIDES - PREPARATION AND STRUCTURE OF OXY TELLURIDES AND DITELLUROLENES OF MOLYBDENUM AND TUNGSTEN [J].

FLOMER, WA ;

KOLIS, JW .

INORGANIC CHEMISTRY, 1989, 28 (13) :2513-2517

[6] ADDITION OF ACTIVATED ACETYLENES TO COORDINATED POLYSULFIDE LIGANDS .2. SYNTHESIS OF THE FE2[S2C2(COOCH3)2]4(2-) DITHIOLENE COMPLEX BY THE ADDITION OF CH3OOCC=CCOOCH3 TO THE (FE2S12)(2-) ANION - CRYSTAL AND MOLECULAR-STRUCTURE OF (PH4P)2FE2[S2C2(COOCH3)2]4 [J].

KANATZIDIS, MG ;

COUCOUVANIS, D .

INORGANIC CHEMISTRY, 1984, 23 (04) :403-409

[7] PHASE ANNEALING IN SHELX-90 - DIRECT METHODS FOR LARGER STRUCTURES [J].

SHELDRICK, GM .

ACTA CRYSTALLOGRAPHICA SECTION A, 1990, 46 :467-473

[8]

SHELDRICK GM, 1997, SHELXTL97 DOS WINDOW

[9] Synthesis, reactivity, and structural characterization of the nonclassical [MTe(7)](n-) anions (M=Ag, Au, n=3; M=Hg, n=2) [J].

Smith, DM ;

Roof, LC ;

Ansari, MA ;

McConnachie, JM ;

Bollinger, JC ;

Pell, MA ;

Salm, RJ ;

Ibers, JA .

INORGANIC CHEMISTRY, 1996, 35 (17) :4999-5006

← 1 →