Evaluation of modified 316L surface properties through HAp suspended EDM process for biomedical application

被引:34
作者
Al-Amin, Md [1 ]
Abdul-Rani, Ahmad Majdi [1 ]
Rana, Masud [2 ]
Hastuty, Sri [3 ]
Danish, Mohd [4 ]
Rubaiee, Saeed [5 ]
bin Mahfouz, Abdullah [6 ]
机构
[1] Univ Teknol Petronas, Dept Mech Engn, Seri Iskandar, Perak, Malaysia
[2] Univ Queensland, Australian Inst Bioengn & Nanotechnol, Brisbane, Qld 4072, Australia
[3] Univ Pertamina, Dept Mech Engn, Jakarta, Indonesia
[4] Univ Jeddah, Dept Mech & Mat Engn, Jeddah 21589, Saudi Arabia
[5] Univ Jeddah, Dept Ind & Syst Engn, Jeddah 21589, Saudi Arabia
[6] Univ Jeddah, Dept Chem Engn, Jeddah 21589, Saudi Arabia
关键词
316L steel; Electro-discharge; HA; Coating; Wettability; Biocompatibility; OF-THE-ART; PROCESS PARAMETERS; ADHESION-STRENGTH; MAGNESIUM ALLOY; DISCHARGE; IMPLANT; BIOMATERIALS; OPTIMIZATION; CORROSION; CRYSTALLINITY;
D O I
10.1016/j.surfin.2021.101600
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Even though the 316L steel is widely utilized in manufacturing biomedical devices including hip joints, screw, plates, and nails, these devices are reported to fail at the early period of implantation caused by inferior bio-logical responses, wear, corrosion, and fatigue. Coating the surface is therefore considered as the underlying factor to mitigate these occurrences. This research aims to evaluate the modified 316L surface through hy-droxyapatite powder (HAp) mixed-electrical discharge process (EDM) for potential bio-implants. Moreover, this study focuses on the parametric effects on the modified surface responses. To synthesize a biocompatible and hard coating, HAp was added in the mineral oil. Several surface characterization methods including Profil-ometer, Goniometer, Scanning-electron microscope (SEM), powder X-ray diffraction (XRD), Energy dispersive X -Ray (EDX), Atomic force microscope (AFM), Vicker's hardness, and biocompatibility test were carried out in this study. The morphological analysis reveals a few micro-cracks formation with shallow craters and nanopores. The elemental analysis confirms Ca, O, P, C, and Ti presence on the machined surface, which replace Fe, Ni, and Cr. A uniform thin coating of 15.29 mu m attributing biocompatible oxides, hydrophilicity, and nano-scale SR of 18.9 nm is obtained. Formation of the hard carbides improves surface microhardness by about 80%. The modified specimen attribute s to a high biocompatibility due to the desired Ca-P based oxides formation. The proposed method can be used for processing 316L steel for a long-term success as the bio-implants.
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页数:13
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