A New Ultrasonic Synthetic Method for Proton Transfer Compound of 2,6-Pyridinedicarboxylic Acid and 2,6-Pyridinediamine

被引：0

作者：

Cai, Mengjun ^{[1
]}

Chen, Jianding ^{[1
]}

机构：

[1] E China Univ Sci & Technol, Natl Engn Res Ctr Ultrafine Powder, Sch Mat Sci & Engn, Shanghai 200237, Peoples R China

来源：

CHINESE JOURNAL OF ORGANIC CHEMISTRY | 2010年 / 30卷 / 07期

关键词：

2,6-pyridinedicarboxylic acid; 2,6-pyridinediamine; proton transfer compound; ultrasonic synthesis; RAY CRYSTAL-STRUCTURE; SELF-ASSEMBLING SYSTEM; PYRIDINE; COMPLEX;

D O I：

暂无

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A new method for synthesizing proton transfer compound [pyda center dot H-2](2+)[pydc](2-) from 2,6-pyridinedicarboxylic acid (pydc center dot H-2) and 2,6-pyridinediamine (pyda) was explored under ultrasonic. Some factors on the yields of proton transfer compound [pyda center dot H-2](2+)[pydc](2-) were investigated including different solvents, reaction time and reactant concentration. The results indicated that the proton transfer compound [pyda center dot H-2](2+)[pydc](2-) could be synthesized in different types of solvents within a relatively short time under ultrasonic. The synthetic method was very convenient without catalyst and heating but short reaction time and high yield.

引用

页码：1076 / 1079

页数：4

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