Controlling the particle size of nanobrookite TiO2 thin films

被引：18

作者：

Arier, Umit Ozlem Akkaya ^{[1
,2
]}

Tepehan, Fatma Zehra ^{[2
]}

机构：

[1] Mimar Sinan Fine Arts Univ, Dept Phys, TR-34349 Istanbul, Turkey

[2] Istanbul Tech Univ, Dept Phys, TR-34469 Istanbul, Turkey

来源：

JOURNAL OF ALLOYS AND COMPOUNDS | 2011年 / 509卷 / 32期

关键词：

TiO2; Nanobrookite; Thin films; Particle size; Sol-gel; PURE BROOKITE; SOL; NANOPARTICLES; DEGRADATION; CALCINATION; TEMPERATURE; HYDROLYSIS; WATER;

D O I：

10.1016/j.jallcom.2011.05.112

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

In this study, pure nanobrookite TiO2 thin films were successfully deposited on glass substrates with the spin-coating method using titanium butoxide and acetic acid. The particle size of TiO2 films was controlled by the water: AcAc volume ratio. This study shows that it is possible to obtain single oriented pure brookite films. The structural and optical properties of the nanobrookite TiO2 thin films were characterized by X-ray diffraction (XRD), atomic force microscopy (AFM), ultraviolet-visible spectroscopy (UV-vis), scanning electron microscopy (SEM), spectrophotometer (NKD), and Fourier transform infrared spectrometer (FTIR). (C) 2011 Elsevier B. V. All rights reserved.

引用

页码：8262 / 8267

页数：6

共 44 条

[41] Effect of stabilizer on structural, optical and electrochemical properties of sol-gel derived spin coated TiO2 films [J].