共 37 条
Influence of the synthesis parameters of TiO2-SBA-15 materials on the adsorption and photodegradation of rhodamine-6G
被引:61
作者:
De Witte, K.
[1
]
Busuioc, A. M.
[2
]
Meynen, V.
[1
,3
]
Mertens, M.
[3
]
Bilba, N.
[2
]
Van Tendeloo, G.
[4
]
Cool, P.
[1
]
Vansant, E. F.
[1
]
机构:
[1] Univ Antwerp VIB, Lab Adsorpt & Catalysis, B-2610 Antwerp, Belgium
[2] Alexandru Ioan Cuza Univ, Iasi 700506, Romania
[3] Flemish Inst Technol Res VITO, B-2400 Mol, Belgium
[4] Univ Antwerp, EMAT, B-2020 Antwerp, Belgium
关键词:
titania;
silica;
photocatalysis;
in situ synthesis;
adsorption;
structure;
D O I:
10.1016/j.micromeso.2007.09.035
中图分类号:
O69 [应用化学];
学科分类号:
081704 ;
摘要:
Ti-SBA-15 mesoporous molecular sieves were prepared following an in situ method. Titania was therefore added during the synthesis of SBA-15. The influence of the silica source, the titania source, the synthesis temperature and the ageing temperature are investigated. These influences are discussed towards structural features, porous characteristics and catalytic performance of the combined titania-silica materials. The catalysts were characterized with Fourier transform-infrared spectroscopy (FT-IR), Raman spectroscopy, electron probe micro analysis (EPMA), nitrogen sorption and X-ray diffraction. The catalytic performance was evaluated using UV-vis spectroscopy in a liquid phase photodegradation reaction. (c) 2007 Elsevier Inc. All rights reserved.
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页码:100 / 110
页数:11
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