Preparation and Characterization of p-Phenylenediamine Supported on Nanocellulose (PDA@CNC) as Novel Recyclable Nano Catalyst for Synthesis of Spiropyran Oxide Derivatives

被引：5

作者：

Song, Congcong ^{[1
]}

Zhang, Zhaogui ^{[1
]}

Shi, Nana ^{[1
]}

Mohammadnia, Majid ^{[2
]}

机构：

[1] Weifang Engn Vocat Coll, Coll Appl Chem Food & Drug, Qingzhou, Shandong, Peoples R China

[2] Islamic Azad Univ, Bojnord Branch, Dept Chem, Young Researcher & Elite Club, Bojnourd, Iran

来源：

POLYCYCLIC AROMATIC COMPOUNDS | 2022年 / 42卷 / 09期

关键词：

p-Phenylenediamine; nanocellulose; spiropyran oxide; isatin; malononitrile; 1; 3-dicarbonyl compound; ONE-POT SYNTHESIS; 3-COMPONENT SYNTHESIS; SPIROOXINDOLE DERIVATIVES; MULTICOMPONENT SYNTHESIS; EFFICIENT; NANOPARTICLES; CELLULOSE; NANOCATALYST;

D O I：

10.1080/10406638.2021.1974895

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

In this study, p-Phenylenediamine supported on nanocellulose (PDA@CNC) was designed. The prepared nanocatalyst was characterized with various analytical techniques such as FT-IR, XRD, TGA, SEM, and CHN. Nanocatalyst used for the synthesis of spiropyran oxide derivatives by designing a simple and efficient method using a three-part reaction between the Isatin derivatives, Malononitrile or Ethyl cyanoacetate and 1,3-dicarbonyl compound. Simple procedure, high yields, short reaction time and environmentally benign method are advantages of this protocol. The nanocatalyst was readily separated by filter and reusable without significant loss of its catalytic efficiency.

引用

页码：6101 / 6111

页数：11

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