Preparation of Palm Oil Based Carbon Nanotubes at Various Ferrocene Concentration

被引:14
作者
Azmina, M. S. [1 ]
Suriani, A. B. [1 ]
Falina, A. N. [1 ]
Salina, M. [3 ]
Rosly, J. [1 ]
Rusop, M. [2 ,3 ]
机构
[1] Univ Pendidikan Sultan Idris, Dept Phys, Fac Sci & Math, Tanjung Malim 35900, Malaysia
[2] Inst Sci, NANO SciTech Ctr, Shah Alam, Malaysia
[3] Univ Teknol MARA, Fac Elect Engn, Solar Cell Lab, Shah Alam 40450, Malaysia
来源
NANOMATERIALS: SYNTHESIS AND CHARACTERIZATION | 2012年 / 364卷
关键词
Nanotubes; Chemical vapor deposition; Scanning transmission electron microscopy; Thermogravimetric analysis and Infrared (IR) Spectroscopy; GROWTH;
D O I
10.4028/www.scientific.net/AMR.364.408
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
In this work, different ferrocene concentration (1.0-8.0 wt%) of bio-hydrocarbon palm oil precursor were utilized to investigate its effect on the characteristics of the produced carbon nanotubes (CNT). The palm oil-ferrocene mixture was vaporized at 450 degrees C and pyrolyzed at 800 degrees C for 30 min time in argon ambient. The CNT were analyzed using field emission scanning electron microscopy, scanning transmission electron microscopy, fourier transform infrared spectroscopy (FTIR) and thermogravimetric analysis. The analysis confirmed different diameter and morphologies of CNT were formed when different ferrocene concentration were used. FTIR spectra show the prominent peak at similar to 1445, 1736, 2851 and 2925 cm(-1) that are identified as CNT and C H-x respectively.
引用
收藏
页码:408 / +
页数:2
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