Electrochemical fluorination: state of the art and future tendences

被引：26
作者：
Conte, L [1 ]
Gambaretto, GP [1 ]
机构：
[1] Univ Padua, Dipartimento Proc Chim Ingn, I-35100 Padua, Italy
来源：
JOURNAL OF FLUORINE CHEMISTRY | 2004年 / 125卷 / 02期
关键词：
electrochemical fluorination; simons process; perfluorodimorpholinepropane;
D O I：
10.1016/j.jfluchem.2003.07.002
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
A brief survey of the ECF process for the preparation of perfluorinated organo-compounds is given. The yield of perfluorinated products depends on the experimental conditions and on the nature of the starting material. Some useful rules are reported in order to optimise the ECF process. An improved operational technique allowed to obtain high yield of perfluorodimorpholinepropane (PFDMP) by simultaneous fluorination of dimorpholinepropane and N-methylmorpholine. (C) 2003 Elsevier B.V. All rights reserved.
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页码：139 / 144
页数：6
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